The invention discloses a 
blue light CdSe 
nanosheet crystal form regulation and control method. According to the 
blue light CdSe 
nanosheet crystal form regulation and control method, 
reaction temperature is reduced, and reaction time is prolonged based on conventional 
blue light CdSe 
nanosheet synthesis, wherein the CdSe nanosheet is prepared through adding of 
cadmium acetate dihydrate, 
selenium powder, and 
oleic acid into 
octadecene (ODE), and degrassing at 
inert atmosphere. The advantages are that: accurate regulation and control of 
reaction temperature and reaction time are adopted, so thatstructure mutual conversion of synthesized nanosheet between face centered cubic 
zinc blende structure and hexagonal wurtzite structure is realized, and nanosheet 
crystal structures, emission peaks,and sizes can be adjusted and controlled preferably; and in addition, Se-ODE is taken as the 
selenium source in conventional wurtzite synthesis technology, in the blue light CdSe nanosheet crystal form regulation and control method, Se 
powder is taken as a 
selenium instead of Se-ODE, Se-ODE synthesis time is about 6h, when Se 
powder is adopted, reaction time is only 3min to 1h, and unreacted Se powder can be precipitated directly, so that 
centrifugation purification is more convenient.