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55 results about "Structural evolution" patented technology

Method for preparing iron oxide red hybridization pigment by means of clay minerals

The invention discloses a method for preparing an iron oxide red hybridization pigment by means of clay minerals. According to the method, natural clay minerals are dispersed in water to form suspension liquid after being subjected to breaking, double rolling and ball milling, molysite and auxiliaries are then added, evenly dispersed and transferred into a hydrothermal reaction kettle, pH of the solution is controlled to be 0.5-4, reaction lasts for 5-60 h at the pressure of 2-8 MPa and the temperature of 160-300 DEG C, and programmed cooling is conducted at the rate of 10 DEG C/min to indoor temperature; the solid product is separated, washed, dried and smashed to generate the bright red hybridization pigment. Structural evolution and recombination are induced through hydrothermal reaction, reaction parameters are precisely controlled, exchange is conducted between Fe3+ and ions in clay minerals under the action of auxiliaries, in-situ formation of a crystalline phase is achieved, the novel silicon-aluminum iron oxide red hybridization pigment with bright color, high stability and uniform size is obtained, and the cost-effective red hybridization pigment is provided for multiple fields including coating, paint, ceramic and ink.
Owner:LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Constant width film stretching device combined with X-ray scattering, and experimental method thereof

The invention provides a constant width film stretching device combined with X-ray scattering, and an experimental method thereof. The device employs two Yaskawa servo motors to drive a ball screw to stretch a sample. The rotation of the motors is controlled by a Labview software. One end of the device is configured to a tension sensor for tracking tension change during a stretching process. During the stretching process, scissor mechanism fixtures are employed perpendicular to the stretching direction, so as to guarantee that the width of the sample can be kept constant during the stretching process and chuck points move uniformly along with the sample. The device employs a forced nitrogen stream to equalize temperature distribution in a sample cabin and reduce thermal degradation of the sample at a high temperature. Two temperature monitoring points are pre-set in the sample cabin. The temperature is precisely controlled by the temperature controller. The device has the advantages of easy disassembly and assembly and the like, is very suitable for combination with synchrotron radiation line stations, and is a very good device for studying the relationship between a structural evolution behavior and the film properties in film stretching and processing.
Owner:UNIV OF SCI & TECH OF CHINA +4

Method for acquiring mobility parameter of re-crystallized structure evolution crystal boundary of metal material

The invention relates to a method for acquiring a mobility parameter of a re-crystallized structure evolution crystal boundary of a metal material. The method comprises the following steps: (1) performing static re-crystallization or dynamic re-crystallization physical thermal simulation test on a metal material sample; (2) acquiring an average grain size of static re-crystallization or dynamic re-crystallization of the sample by utilizing a microstructure representation test; (3) establishing a re-crystallization dynamical model on the basis of a structural evolution numerical simulation method, wherein the model includes nucleation and growing sub-models; (4) describing a nucleation rate sub-model through a nucleation rate, excluding the parameters, such as nucleation activation energy, difficult to acquire through the test and the parameters without physical significance; (5) expressing the migration rate of the crystal boundary of a re-crystallization growing sub-model by the product of the driving force and the mobility parameter of the crystal boundary, wherein the mobility parameter of the crystal boundary is a unique fitting parameter in the whole model; (6) adjusting the mobility parameter of the crystal boundary by adopting an inverse optimization algorithm, comparing a numerical simulation result with a test result and confirming the parameter when a difference between the numerical simulation result with the test result is less than a threshold value (0.01-0.1).
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Method for quantitatively determining brittle-ductile critical condition of gypsum rock-carbonatite

The invention provides a method for quantitatively determining the brittle-ductile critical condition of gypsum rock-carbonatite. The method comprises the steps that the gypsum rock-carbonatite is adopted as a sample, and the sample comprises the lithological characters of gypsum containing dolomite, gypseous dolomite, dolomite-quality gypsum rock and dolomite containing gypsum rock; temperature and pressure of a critical construction period of petroleum entrapment evolution according to the history of structural evolution of a basin where the gypsum rock-carbonatite is located, and are adopted as temperature and pressure of experimental simulation; the maximum differential stress value and the maximum inflection point stress point of the sample are measured under simulation temperature and pressure respectively; the critical position of conversion of the brittleness and tenacity of the sample is quantitatively evaluated according to the maximum differential stress value and the maximum inflection point stress point of the sample, and the brittle-ductile critical condition of the gypsum rock-carbonatite is quantitatively determined. According to the method, the brittle-ductile critical condition of the gypsum rock-carbonatite can be accurately evaluated, and a basis is provided for accurately evaluating and predicting petroleum entrapment of the gypsum rock-carbonatite.
Owner:PETROCHINA CO LTD

Method for determining time series of oil and gas charging in ore-bearing formations of shallow layer of basin margin

The invention belongs to the technical field of a sandstone-type uranium deposit in a basin, and specifically discloses a method for determining a time series of oil and gas charging in ore-bearing formations of a shallow layer of a basin margin. The method comprises the following steps: (1) determining a working area and a target layer, and determining the target layer geologic age range is t0-t0'; (2) performing a sample collection in a circled work area; (3) selecting apatite and extracting a chloroform pitch A from the collected samples; (4) performing a inversion of a history of structural evolution and an oil source analysis on the sample, and screening a sample having a common single source; (5) performing the organic matter Re-Os dating of the chloroform pitch A on the homologous and single source sample, comparing an obtained age data tn with the age t0 of the formation target layer, and retaining the age of tn<=t0; and obtaining the oil and gas charging time (t) order according to whether the retention age is in a strong tectonic activity period. The method can accurately identify the period and time of the oil and gas charging in a prospecting target layer of a shallow layer of a petroliferous basin margin.
Owner:BEIJING RES INST OF URANIUM GEOLOGY

Shale gas multi-factor area selection and evaluation method based on fuzzy matrix

InactiveCN107589236ASolve the technical problems of constituency evaluationSpeed up constituencyEarth material testingGeological measurementsKinematicsStructural evolution
The invention discloses a shale gas multi-factor area selection and evaluation method based on fuzzy matrix. The method comprises the following steps: step one, studying the geometric features, formation mechanism, and basin properties of basin controlling fracture, and establishing a static geologic model; step two, studying the kinematics features of basin controlling fracture, and analyzing thehistory of structural evolution, burial history of shale, and hydrocarbon generation history of shale; step three, extracting shale static/kinetic evaluation features, defining various parameters ofthe shale gas area selection and evaluation, and assigning the parameters; step four, establishing a fuzzy matrix, and carrying out multi-factor evaluation; and step five, determining the prospectivearea and favorable area based on the results of shale gas area selection and evaluation. The multi-factor area selection and evaluation method has the advantages that various static/kinetic parametersduring the shale gas formation and enrichment process are integrated, a mathematic method based on a fuzzy matrix is used to carry out area selection and evaluation, the artificial interference is reduced maximally, and the method has an important meaning for the shale gas area selection and exploration.
Owner:OIL & GAS SURVEY CGS

Method for evaluating favorable reservoir formation zone of ancient buried hill

ActiveCN110443719AEvaluation validity is reliableImprove accuracyResourcesGeomorphologyContact time
The invention relates to a method for evaluating a favorable reservoir formation zone of an ancient buried hill. The evaluation method comprises the following steps: determining a zone where high-quality source rock develops in a basin and a stratum position where the high-quality source rock is located; determining the main hydrocarbon expulsion threshold depth of the high-quality source rock; determining the current ancient buried hill structure characteristics of the basin according to the seismic profile structure interpretation result; constructing evolution profiles of the basin in different periods to research the evolution history of the ancient buried hill, determining the thickness of the layer, in lateral contact with the ancient buried hill, of the high-quality source rock contained in the depth range of the main hydrocarbon expulsion threshold, determining the lateral contact time of the high-quality source rock in different layers and the ancient buried hill, and establishing the reservoir forming probability of the ancient buried hill and favorable zone optimization. According to the evaluation method, the reservoir forming probability of the ancient buried hill is evaluated by researching the effective contact area and time period of the ancient buried hill and high-quality source rock according to the development characteristics of the ancient buried hill in different structural evolution periods in combination with the main hydrocarbon expulsion threshold depth of the high-quality source rock, so that optimal evaluation of the basin ancient buried hill iscarried out.
Owner:CHINA PETROLEUM & CHEM CORP +1

Device and method for estimating soil structural evolution online in real time based on unmanned aerial vehicle

The invention discloses a device and method for estimating soil structural evolution online in real time based on an unmanned aerial vehicle; the device comprises the unmanned aerial vehicle, a telescopic device, a micro-distance video and image acquisition device, a first signal receiver, a second signal receiver, and a remote control computer; the method comprises: first, establishing a micro-distance video gray image database; second, establishing in the database, a correspondence between substances and a gray value range; third, calculating in the micro-distance video gray image, a number of pixels representative of the substances in the gray value range, and establishing a relation with corresponding substance contents or forms; fourth, determining actual characteristic parameters of a soil body to be detected according to the above relation so as to determine development state of the soil body. Micro-distance video estimation is performed on a soil sample in situ, testing precision is high, and soil body composition and its evolution identification are more accurate; it is possible to perform large-range long-term continuous real-time online monitoring for a soil body where a human body and an axle-driven vehicle cannot reach easily, and evolution law of the soil body in the area is obtained.
Owner:WUHAN UNIV

Analysis and evaluation method for structural evolution of DNAPL contaminated cohesive soil

The invention discloses an analysis and evaluation method for structural evolution of DNAPL contaminated cohesive soil. The method comprises the following steps: determining environmental basic data of a target site; collecting a pollution-free cohesive soil undisturbed soil sample and a DNAPL polluted cohesive soil undisturbed soil sample in the target soil layer; respectively cutting the obtained undisturbed soil sample into pollution-free cohesive soil particles and DNAPL polluted cohesive soil particles with sizes required by an electron microscope scanning test and a mercury injection test, and carrying out freeze drying; then carrying out an electron microscope scanning test on the pollution-free cohesive soil particles and the DNAPL polluted cohesive soil particles; carrying out a mercury injection experiment on the freeze-dried pollution-free cohesive soil particles and DNAPL polluted cohesive soil particles; and according to the results of an electron microscope scanning testand a mercury injection test, analyzing the microstructure change of cohesive soil so as to evaluate influence of the cohesive soil on pollutant migration. The method has the advantages that the cohesive soil before and after DNAPL pollution is studied through electron microscope scanning and mercury injection experiments, and the method has significance in mastering microstructure evolution and migration characteristic changes caused by interaction of the cohesive soil and organic pollutants.
Owner:SHANGHAI GEOTECHN INVESTIGATIONS & DESIGN INST

High-performance fiber drying detection testing machine

ActiveCN101871860ADetecting Structural EvolutionOvercome the lack of guaranteed qualityPreparing sample for investigationFiberDry box
The invention provides a high-performance fiber drying detection testing machine which comprises a stand, a drying mechanism, a winding mechanism and a translation mechanism; the drying mechanism comprises a drying box body, a heating box, a silk supporting roller, a return air pipe, a fan and a pressure-equalizing box; a box door which is provided with a testing port is installed on the front surface of the drying box body; a return air inlet and the pressure-equalizing box are respectively arranged at the top and the bottom of the drying box body; a pressure-equalizing distribution outlet net plate and a static-pressure distribution inlet net plate are arranged above the pressure-equalizing box; the winding mechanism is installed at one side of the silk outlet of the drying box body; and the translation mechanism is used for the horizontal movement of the drying box body. The invention has reasonable structure and convenient operation, can be matched with a synchrotron radiation device, can accurately detect the structural evolution condition of a high-performance fiber silk bundle in the drying process in time, supplies a strong technical support for the drying process design of high-performance fiber production, and overcomes the defects that the debugging period of a trial and error method is long and the fiber quality can not be ensured.
Owner:JIANGSU SHENTAI SCI & TECH DEV

Experimental device and method for carrying out simulation study on heat exchange and geometric structural evolution of foam fracturing fluid in fracture passage

The invention discloses an experimental device and method for carrying out simulation study on heat exchange and geometric structural evolution of foam fracturing fluid in a fracture passage. The experimental device comprises a solution storage box, a gas cylinder, a foam generator, a fracture simulation device and a recorder, wherein the solution storage box is used for storing aqueous solution of a surfactant; the gas cylinder is used for storing and supplying gas for generating foam; the foam generator is used for generating the foam; the fracture simulation device is transparent; a passageis formed in the fracture simulation device and used for simulating a stratum fracture with heat flow; both a width and an inclination angle of the passage for simulating the stratum fracture are adjustable; a heating plate is arranged in the passage for simulating the stratum fracture; a plurality of thermocouples are arranged on the heating plate; and the recorder is used for recording data acquired by the thermocouples. The experimental device and method disclosed by the invention can simulate to carry out study on multi-phase flowing and convective heat exchange characteristics of the foam fracturing fluid with different parameters in the stratum fractures with different widths and inclination angles.
Owner:XI AN JIAOTONG UNIV

Method for in-situ study of amorphization mechanism of germanium-antimony-tellurium material under electron beam irradiation

The invention discloses a method for in-situ study of an amorphization mechanism of a germanium-antimony-tellurium material under electron beam irradiation. The method comprises the following steps: selecting a germanium-antimony-tellurium crystal thin film of which the surface is deposited on a carbon supporting film copper carrying net with a standard size of a transmission electron microscope;carrying out surface pretreatment on the prepared film sample by adopting a plasma cleaning technology, and carrying out plasma cleaning by selecting argon; placing a pretreated electron microscope sample in the transmission electron microscope, and searching an area which is smooth in surface, free of carbon deposition, pollution and damage and uniform in thickness in the thin film sample to serve as an irradiation area; setting irradiation parameters, and inducing the material to be gradually amorphized; and observing and recording the evolution process of the amorphous structure of the material in situ, and analyzing the amorphous phase change mechanism of the material. According to the method, the gradual amorphization of the germanium-antimony-tellurium material is realized through electron beam irradiation, and the structural evolution process of the material amorphization is directly observed and analyzed by virtue of the transmission electron microscope, so that the convenientresearch method and a reliable experimental basis are provided for exploring the amorphization mechanism of the germanium-antimony-tellurium material.
Owner:XI AN JIAOTONG UNIV

A Method for Obtaining Mobility Parameters of Grain Boundary in Metal Material Recrystallization Microstructure Evolution

The invention relates to a method for acquiring a mobility parameter of a re-crystallized structure evolution crystal boundary of a metal material. The method comprises the following steps: (1) performing static re-crystallization or dynamic re-crystallization physical thermal simulation test on a metal material sample; (2) acquiring an average grain size of static re-crystallization or dynamic re-crystallization of the sample by utilizing a microstructure representation test; (3) establishing a re-crystallization dynamical model on the basis of a structural evolution numerical simulation method, wherein the model includes nucleation and growing sub-models; (4) describing a nucleation rate sub-model through a nucleation rate, excluding the parameters, such as nucleation activation energy, difficult to acquire through the test and the parameters without physical significance; (5) expressing the migration rate of the crystal boundary of a re-crystallization growing sub-model by the product of the driving force and the mobility parameter of the crystal boundary, wherein the mobility parameter of the crystal boundary is a unique fitting parameter in the whole model; (6) adjusting the mobility parameter of the crystal boundary by adopting an inverse optimization algorithm, comparing a numerical simulation result with a test result and confirming the parameter when a difference between the numerical simulation result with the test result is less than a threshold value (0.01-0.1).
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Constant width film stretching device combined with X-ray scattering, and experimental method thereof

The invention provides a constant width film stretching device combined with X-ray scattering, and an experimental method thereof. The device employs two Yaskawa servo motors to drive a ball screw to stretch a sample. The rotation of the motors is controlled by a Labview software. One end of the device is configured to a tension sensor for tracking tension change during a stretching process. During the stretching process, scissor mechanism fixtures are employed perpendicular to the stretching direction, so as to guarantee that the width of the sample can be kept constant during the stretching process and chuck points move uniformly along with the sample. The device employs a forced nitrogen stream to equalize temperature distribution in a sample cabin and reduce thermal degradation of the sample at a high temperature. Two temperature monitoring points are pre-set in the sample cabin. The temperature is precisely controlled by the temperature controller. The device has the advantages of easy disassembly and assembly and the like, is very suitable for combination with synchrotron radiation line stations, and is a very good device for studying the relationship between a structural evolution behavior and the film properties in film stretching and processing.
Owner:合肥中科优材科技有限公司

Method and device for determining dynamic change process of ancient karst diving surface

The invention provides a method and device for determining the dynamic change process of an ancient karst diving surface, and the method comprises the steps: determining the structural evolution history of a target layer of a research area, and determining the lifting of the ancient karst diving surface of the target layer in a supergene karst period; establishing an ancient karst zone identification and division template; according to the ancient karst zone identification and division template, carrying out different single well vertical ancient karst zone division in a research area, and determining an earth surface karst zone, a vertical seepage zone, a transition zone, a horizontal subsurface flow zone and a deep slow flow zone in each well; dividing a single transition zone in the transition zone, identifying the ancient karst phreatic surface, and determining the vertical change process of the ancient karst phreatic surface of a single well; well-connected karst zone comparison is carried out, and the lateral distribution range of the ancient karst phreatic water surface in the same period is analyzed; and in combination with the ancient karst landform, analyzing the relationship between the ancient karst phreatic surface and the ancient karst landform, determining the longitudinal development position and the transverse distribution range of the ancient karst phreatic surface in different periods, and determining the dynamic change process of the ancient karst phreatic surface.
Owner:PETROCHINA CO LTD
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