The invention discloses a method for preparing a magnetic P-type
molecular sieve by using
coal gangue. The method comprises: 1,
grinding coal gangue, and carrying out high temperature calcining activating on the grinded
coal gangue by using
sodium carbonate; 2, oxidizing at a low temperature, adding
hydrochloric acid, soaking, and filtering; 3, preparing an iron-doped
molecular sieve from the
filtration residue and the filtrate obtained after the
filtration; and 4, placing the iron-doped
molecular sieve in a porcelain boat, placing the porcelain boat in a tubular furnace, introducing
nitrogen into the
tube furnace, introducing
hydrogen after the air in the tubular furnace is completely discharged, heating to a temperature of 650-700 DEG C, continuously carrying out a reduction reaction for 2-3 h, introducing
nitrogen after completing the reaction, and cooling to a
room temperature to obtain the magnetic P-type molecular
sieve. According to the present invention, the
coal gangue is used as the
raw material, the Fe<3+>
dissolution is performed with
hydrochloric acid and is complexed by adding
oxalic acid, and finally high temperature reduction is performed to prepare the magnetic P-type molecular
sieve; the magnetic P-type molecular
sieve has characteristics of high specific surface area and strong adsorption performance; and the magnetic P-type molecular sieve is easy to separate and recover through the external
magnetic field, and the problem of high cost of the molecular sieve synthesis is solved.