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359 results about "Engineering production" patented technology

Production engineering is a combination of manufacturing technology, engineering sciences with management science. A production engineer typically has a wide knowledge of engineering practices and is aware of the management challenges related to production.

Large blocked TS-1 molecular sieve with high catalytic activity and synthetic method thereof

The invention relates to a large blocked TS-1 molecular sieve with high catalytic activity and a synthetic method thereof, belonging to the technical fields of catalytic chemistry and chemical engineering. The large blocked TS-1 molecular sieve is a titanium-silicalite molecular sieve which has an MFI structure and formed by mutually piling nano-level TS-1 crystal grains with the blocked size of 20-100 micrometers and the mesoporous volume of 0.55cm<3>/g. The large blocked TS-1 molecular sieve is formed by evenly mixing tetraethoxysilane as a silicon source, tetrabutyl titanate as a titanium source, tetrapropylammonium hydroxide as a template agent, water and isopropanol as a solvent and H2O2 as an inorganic additive and carrying out hydrothermal crystallization on the mixture at a temperature between 160 DEG C and 180 DEG C for 6-96 hours. The large blocked TS-1 molecular sieve maintains a single crystal grain nano-size structure, has favorable catalytic reaction activity and can realize the separation on the entire device by filtering operation; and the adopted inorganic addictive H2O2 is friendly to the environment and has low price, thus the invention has important significance in the practical chemical engineering production.
Owner:JILIN UNIV

Technique method for producing sodium bisulfide

The invention discloses a technique method for producing sodium bisulfide and belongs to the technical field of the chemical engineering production technology. The technique method for producing sodium bisulfide is low in production cost and can control product quality easily during production. The technique method includes: feeding buffered hydrogen sulfide and process absorption liquid with sodium sulphide as the main ingredient into an absorption tower respectively from the lower portion and the upper portion of the absorption tower, absorbing the hydrogen sulfide and the process absorption liquid on the surface of packing in the absorption tower to generate solution with the sodium bisulfide as the main ingredient, enabling the solution to flow to the bottom of the absorption tower, and discharging the unabsorbed hydrogen sulfide tail gas from the top of the absorption tower; pumping the solution at the bottom of the absorption tower out, returning most of the solution back to the absorption tower for recycling, feeding the small amount of solution to a sodium bisulfide production solution storing tank, and simultaneously adding the process absorption liquid in the absorption tower from the upper portion of the absorption tower during the absorption circulating process; and finally performing evaporation, concentration and dehydration on the solution, cooling the solution for molding, packaging and finishing the production of the sodium bisulfide.
Owner:CHENGDU DEMEI ENG TECH

Production process for preparing calcium oxide and sulfur dioxide by decomposing ardealite

The invention belongs to the technical field of environmental protection treatment and chemical engineering production, and relates to a production process for preparing calcium oxide and sulfur dioxide by decomposing ardealite. The process comprises the following steps of: mixing the ardealite and charcoal according to a dry weight ratio of 10-20:1, granulating the mixture to obtain particles of which the particle size is between 1 and 4mm, drying and dewatering the particles, putting the particles in a fluidized bed decomposing furnace to be directly contacted with high-temperature furnace gas for reaction for 15 to 50 minutes at a temperature of between 1,000 and 1,300 DEG C, and generating the sulfur dioxide gas and the calcium oxide. The process can solve the problem of comprehensively utilizing waste residues of ardealite, the content of SO2 in the discharged tail gas is high enough to be used for producing sulfuric acid, and the calcium oxide which is a byproduct can be used in various industries such as construction, road, aquaculture and the like, so that the process meets the requirements on the scientific outlook on development; moreover, compared with the process for co-production of cement by sulfuric acid prepared by the ardealite, the process greatly saves investment and electric consumption.
Owner:SINOPEC NANJING ENG & CONSTR

Preparation method of nitrogen/ sulphur co-doping three-dimensional graphene sponge

The invention relates to a preparation method of a nitrogen/ sulphur co-doping three-dimensional graphene sponge. The preparation method of the nitrogen/ sulphur co-doping three-dimensional graphene sponge comprises the steps of firstly, fully dispersing a graphene oxide and thiourea mixture through an ultrasonic oscillating way, then filling the mixture into a hydrothermal reaction kettle, reducing the graphene oxide into graphene through high temperature and high pressure, meanwhile, self-assembling the graphene into a three-dimensional graphene macroscopic body, and doping a nitrogen element and a sulphur element into a graphene substrate; and finally, repetitively cleaning the three-dimensional graphene macroscopic body, and freeze drying to obtain the nitrogen/ sulphur co-doping three-dimensional graphene sponge. The three-dimensional graphene sponge synthesized through hydrothermal reaction has the advantages of light weight and porosity, and is applied in a lithium-sulfur battery so as to be capable of improving the electrical conductivity of an anode material and solving the problem of big volume change during an electrode reaction process. The preparation method of the nitrogen/ sulphur co-doping three-dimensional graphene sponge provided by the invention is simple and easy to implement, and is very applicable to engineering production.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Full-automatic commercial pure titanium smelting method adopting electron beam cold hearth furnace

The invention relates to a full-automatic TA1 smelting method adopting an electron beam cold hearth furnace and belongs to the technical field of production engineering application. The production method comprises the following steps: drying and putting titanium sponge into an Archimedean screw tube which is mounted into a feeding system of an electron beam cold hearth melting furnace (EB furnace for short), wherein different rotary speeds are set; when the degree of vacuum of the feeding system reaches 0.4-0.8 Pa and the degree of vacuum of a main smelting cold hearth reaches 0.05-0.8 Pa, starting the feeding system to feed the titanium sponge into the smelting cold hearth of a main smelting chamber; triggering an electron gun to melt the titanium sponge into liquid titanium which flows through a primary refining cold hearth and a main refining cold hearth and then into a rectangular withdrawing crucible; controlling the rotary speed of the Archimedean screw tube to control the feeding speed and scanning patterns so as to control the melting speed, and the ingot pulling rate thereby realizing full-automatic control. The method has the advantages of good ingoting quality, high one-step yield, low manufacturing cost, controllable production period, simplicity in operation, energy conservation, environmental protection and high repeatability.
Owner:YUNNAN TITANIUM IND

Vanadium/copper solid solution transition connection-based welding process for titanium-containing metal layer/pipeline steel layer composite board

The invention discloses a vanadium/copper solid solution transition connection-based welding process for a titanium-containing metal layer/pipeline steel layer composite board. The titanium-containing metal layer/pipeline steel layer composite board is formed in the way that an industrial pure titanium and titanium alloy board and a pipeline steel board are connected together by the explosive welding process and the connected boards are rolled by use of the controlled rolling and controlled cooling technology, so that an industrial pure titanium and titanium alloy layer is arranged on one side of the titanium-containing metal layer/pipeline steel layer composite board, and a pipeline steel layer is arranged on the other side. The welding process provided by the invention is simple in process implementation, can realize metallurgical butt-welding engineering production of the titanium-containing metal layer/pipeline steel layer composite board, enables a metallurgically connected seam to be relatively good in appearance and favorable in mechanical property index, and achieves reliable connection of the titanium-containing metal layer/pipeline steel layer composite board while guaranteeing the decay resistance of the titanium-containing metal layer/pipeline steel layer composite board.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Floating breakwater capable of giving consideration to inner oscillation water column wave energy conversion function and method

The invention discloses a floating breakwater and a method capable of giving consideration to an inner oscillation water column wave energy conversion function. In the floating breakwater capable of giving consideration to the inner oscillation water column wave energy conversion function, the exterior of a floating body is anchored into a seabed through an anchor rope connection sinking block; anoverhauling channel is arranged at the upper part of the floating body; and wave energy conversion related configurations are arranged in the floating body, and comprise an air chamber, an air turbine, a turbine bracket, a linkage shaft, a generator, a cushion layer and an air chamber inner water body. A realization method of the floating breakwater capable of giving consideration to the inner oscillation water column wave energy conversion function comprises the steps of a breakwater arrangement process, a process of the floating body eliminating the wave effect, a wave energy conversion output process and an overhauling process. On the basis of maintaining traditional wave retaining and eliminating functions of the floating breakwater, the wave energy conversion function is realized byusing the oscillation design of water in an air chamber, and the power output in the wave energy conversion process is continuous, so that the reliability is good; the stress design of the breakwateris reasonable, and the durability is excellent; and meanwhile, the construction cost is low, and the engineering production advantages are obvious.
Owner:ZHEJIANG UNIV

Pure titanium or titanium alloy/carbon steel laminar composite plate welding method

The invention discloses a pure titanium or titanium alloy/carbon steel laminar composite plate welding method. A pure titanium or titanium alloy/carbon steel laminar composite plate is formed by metallurgically connecting an industrial pure titanium or titanium alloy plate with a carbon steel plate through explosion and hot rolling processes; a welding groove is finely designed and machined for the composite plate; MAG and TIG fusion welding technologies are combined; the plate-plate butt welding connection is performed for the pure titanium or titanium alloy/carbon steel laminar composite plate by a spraying transition technology; and a spraying layer is excellent in formation, compact and high in bonding force with a lower-layer material, achieves an excellent metallurgy transition connecting effect, and prevents generation of brittle and hard phases in welding lines. The welding method realizes engineering production of metallurgy butt welding connection of the pure titanium or titanium alloy/carbon steel laminar composite plate, is better in appearance and excellent in mechanical performance of metallurgy connection welding lines, guarantees corrosion resistance of the welding lines, and realizes reliable metallurgy connection of the welding lines.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Ferro-cerium-based rapid quenching permanent magnet powder and preparation method of ferro-cerium-based rapid quenching permanent magnet powder

The invention relates to ferro-cerium-based rapid quenching permanent magnet powder and a preparation method of the ferro-cerium-based rapid quenching permanent magnet powder. The alloy composition chemical formula of the ferro-cerium-based rapid quenching permanent magnet powder is [Ce100-x, Rex]aFe100-a-b-cBbTMc, wherein the x is the mass percent of the rare earth gross, the a, the b and the c show the mass percents of corresponding elements respectively, 0<=x<=50%, 27.5%<=a<=32%, 0.8%<=b<=1.5%, 0.5%<=c<=5%, the Re is one or more of Nd, Pr, Dy and Tb, and the TM is one or more of Ga, Co, Cu, Nb and Al. According to the preparation method, the ferro-cerium-based rapid quenching permanent magnet powder and Re'-Fe-B without Ce can be prepared with a water-cooling electromagnetic roller (a copper alloy roller or a molybdenum roller), and a ferro-cerium-based hot-pressing magnet with double hard magnetic principal phases or multiple hard magnetic principal phases can be prepared with the two kinds of magnetic powder. The ferro-cerium-based rapid quenching permanent magnet powder fills up blanks of middle-grade magnet powder and lower-grade magnet powder on the market at present, the product performance cost ratio is high, and the ferro-cerium-based rapid quenching permanent magnet powder and the preparation method are suitable for engineering production.
Owner:CENT IRON & STEEL RES INST

High-temperature high-pressure tubular-flow erosion corrosion experiment device

A high-temperature high-pressure tubular-flow erosion corrosion experiment device mainly includes: a high-temperature high-pressure kettle, a first pressure meter, a temperature meter, a sample test tube, an actual object test tube, a sample trough, a magnetic pump, a liquid transporting pipe, and an ultrasonic flow rate meter. The high-temperature high-pressure kettle is used for providing a fluid at certain temperature and under certain pressure. The actual object test tube is connected to a third joint and a fourth joint of the liquid transporting pipe through a second flange. An actual object tube is fixed in the actual object test tube through a first corrosion-resistant sealing ring. The sample test tube is connected to a first joint and a second joint of the liquid transporting pipe through a first flange. The sample trough, in which a sample is hung, is formed in the sample test tube. The magnetic pump is used for providing power to the experiment device for driving fluid circulation. The ultrasonic flow rate meter is used for testing the speed of the circulated fluid. The whole experiment device is made of corrosion-resistant alloy and a heat insulation layer covers external walls of all parts, so that temperature loss is avoided. The device is suitable for drilling production engineering of petroleum and natural gas.
Owner:SOUTHWEST PETROLEUM UNIV

Forming destructive distillation method for crushed low metamorphic coal powder, asphalt and tar residues

The invention discloses a method of preparing formed semi-coke by using low metamorphic coal powder, asphalt and tar residues as raw materials and belongs to the technical field of coal chemical engineering. The method comprises the following steps: mixing and crushing low metamorphic coal, asphalt and tar residues to obtain raw material powder; pressurizing and forming the raw material powder in a forming mould to obtain molded coal; and pyrolyzing the molded coal in a destructive distillation device to obtain molded semi-coke, coal tar and gas. By taking the coal ash as the raw material, the utilization efficiency is improved, so that the problem that the semi-coke producing raw material is insufficient is solved, and meanwhile, the situation that the coal resource is short is also alleviated; by using asphalt and tar residues as an adhesive, not only is the problem that waste residues generated in the chemical engineering production process cannot be effectively treated and the utilization value is low to realize recycle of the abandoned resource, but also remarkably improves the oil yield of the coal tar. The stability and mechanical strength of the molded coal and the molded semi-coke are remarkably enhanced, and the economical benefit of an enterprise is extremely improved, thereby developing a novel path for semi-coke production.
Owner:YULIN UNIV

Etching liquid for TFT (thin film transistor)array substrate copper conductor

The invention relates to etching liquid for a TFT (thin film transistor)array substrate copper conductor. The etching liquid comprises primary oxidant, secondary oxidant, a chelating agent, inhibitor and additive, wherein the primary oxidant is hydrogen peroxide; the secondary oxidant is phosphoric acid, sulfuric acid and nitric acid; the chelating agent is amino compounds; the inhibitor is aminoimidazole compounds and carboxylic acid compounds; and the additive is amine compounds containing ammonia nitrogen and carboxy oxygen coordination atoms. According to the etching liquid, the characteristic of shorter process windows of the etching liquid for the copper conductors is obviously improved, the engineering control difficulty is reduced, and the stability of engineering production and the output yield are improved by means of the components and the types of the novel chelating agent and the additive; the shelf-time stability is improved, and the stability of the etching performance can be kept in the later shelf-time storage period; and the service life (more than or equal to 5,000 ppm) is prolonged, the process windows are not obviously narrowed in the later processing period, and the properties and the like are relatively stable.
Owner:SHENZHEN CHINA STAR OPTOELECTRONICS TECH CO LTD

Micro-spherical silicon oxide/aluminum oxide based noble metal catalyst and preparation method thereof

The invention provides a micro-spherical SiO2-Al2O3 based noble metal catalyst and a preparation method thereof. The preparation method comprises the following steps: dispersing silica sol into a silica sol system, so that silica sol is mixed with alumina sol and a coagulant to form formed sol, forming the sol by virtue of an atomizing dispersion-oil column formation method, and carrying out aging, washing, drying and roasting to obtain micro-spherical SiO2-Al2O3; and loading noble metal active components with the micro-spherical SiO2-Al2O3 as a carrier, obtain the micro-spherical SiO2-Al2O3 based noble metal catalyst. The catalyst has the characteristics that the specific surface area and the pore volume are large, the dispersity of active components is high, the abrasion index is relatively low, and the wear resistance is high. The catalyst is mainly applied to a hydrogenation process of preparing hydrogen peroxide by using a fluidized bed anthraquinone method and has relatively high catalytic activity, selectivity and stability. The catalyst can be also applied to reaction processes such as hydrorefining, selective hydrogenation and selective oxidation in petrochemical engineering and fine chemical engineering production.
Owner:BEIJING UNIV OF CHEM TECH

Refining method of xylose in hemicellulose hydrolysate

The invention relates to the technical field of chemical engineering production, in particular to a refining method of xylose in hemicellulose hydrolysate. The method comprises the following steps of(1) removing impurities from the hemicellulose hydrolysate; feeding the hemicellulose hydrolysate into an ultrafiltration membrane to obtain transmission liquid; (2) separating the transmission liquidby the nanofiltration membrane; remaining sulfuric acid into concentrated liquid, wherein the transmission liquid contains acetic acid and xylose; (3) performing electrodialysis separation on aceticacid and xylose water solution; (4) directly using the xylose water solution for furfural production; (5) performing extraction and rectification on the acetic acid by solvents to obtain acetic acid with the concentration being 98.5 percent. The method has the advantages that the operation is simple; the obtained xylose water solution can be directly used for the furfural production; the acetic acid with the mass concentration being about 20 percent can be obtained; a solvent extraction rectification device is used for extraction separation to obtain the acetic acid with the mass concentrationbeing 98.5 percent. In the process, the separated sulfuric acid returns to the hydrolysis work procedure to be continuously used; active ingredients are recovered and reused; the production cost is reduced.
Owner:SICHUAN GOLDEN ELEPHANT SINCERITY CHEM CO LTD
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