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104results about How to "Ingenious design ideas" patented technology

Poly-dopamine based porous carbon fiber/MoSe2 composite material and preparation method thereof

The invention belongs to the technical field of a composite fiber material, in particular relates to a poly-dopamine based porous carbon fiber / MoSe2 nanosheet composite material and a preparation method thereof. The method comprises the following steps of preparing a spinning solution with a spinnable high-polymer material, and preparing to obtain porous fiber with an uniform structure by an electrostatic spinning device; immersing the porous fiber in a dopamine solution, and controlling the thickness of a poly-dopamine cladding layer by adjusting the concentration and the reaction time of the dopamine solution; carrying out high-temperature carbonization to achieve carbonization on the poly-dopamine modified porous fiber material; and uniformly arranging MoSe2 nanosheets on the surface of the porous fiber by a hydrothermal method. The method disclosed by the invention is safe and environment-friendly, and the prepared porous carbon fiber / MoSe2 has the advantages of high active substance content, high specific area, high conductivity, stable physical and chemical performance and the like, and is an ideal electrode material for preparing an active electric catalyst for a hydrogen evolution reaction.
Owner:FUDAN UNIV

Carbon nano-tube with fluorine-containing surface and preparation method thereof

The invention discloses a carbon nano-tube with a fluorine-containing surface, wherein the surface of the carbon nano-tube is of a carbon-fluorine covalent bond structure, the content of fluorine in the surface is 4-14%, and the decrease rate of the content of the fluorine is smaller than 5% after a produced fluorocarbon nano-tube is treated for 1 hour under a vacuum condition at 350 DEG C. The preparation method of the carbon nano-tube comprises the following steps of: firstly treating the carbon nano-tube by utilizing strong acid, secondly placing the carbon nano-tube in a vacuum reactor, charging fluorine/inert gas mixture with fluorine partial pressure of 10-100KPa in nitrogen atmosphere under room temperature to react for 0.5-4 hours at 150-300 DEG C, and cooling down to be the room temperature to obtain the carbon nano-tube. The fluorocarbon nano-tube prepared by the preparation method disclosed by the invention has the advantages of high fluorine content, low reaction temperature, high safety, energy conservation, and simple process, a fluorine-containing group of the surface of the treated prepared fluorocarbon nano-tube has good heat resistance and lower cost, and the fluorocarbon nano-tube is suitable for large-batch production and has stronger application prospect.
Owner:SICHUAN UNIV

Physical vapor deposition preparation method for high-entropy alloy film with uniform and controllable components

The invention discloses a physical vapor deposition preparation method for a high-entropy alloy film with uniform and controllable components. The preparation method comprises the steps that a magnetron sputtering technology is adopted, a magnetron sputtering composite target serves as a target material, one or more kinds of gas serve as working gas, negative bias voltage is applied to a base body, and therefore the high-entropy alloy thin film with the uniform and controllable components is obtained on the surface of the base body through deposition; and the magnetron sputtering composite target comprises at least one target period which is periodically arranged in the vertical direction, and each target period comprises single alloy target materials which are sequentially stacked in thevertical direction. According to the provided preparation method, the method is simple, the overall design idea is ingenious, all pure targets are independent of one another and are flexible and convenient to combine, the adjustment can be carried out according to needs, and the high-entropy alloy thin film with the controllable and uniform components can be economically and efficiently prepared;and according to the method, the thin-layer target materials are stacked and spliced together, so that compared with combination of large pure target materials, the method can enable various components in a product to be uniform, so that the product with a single phase is obtained.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Pure carbon fiber material adopting 'vesical string' structure and preparation method of pure carbon fiber material

The invention belongs to the technical field of nano-fiber materials, in particular to a pure carbon fiber material adopting a 'vesical string' structure and a preparation method of the pure carbon fiber material. The preparation method comprises the following steps: preparing a spinning solution from a spinnable polymer material, and preparing nanofibers of uniform structures with an electrostatic spinning device; uploading iron oxide hydroxide cambiform nanorods on the surfaces of the nanofibers uniformly via a water bath or hydrothermal method; soaking an iron oxide hydroxide-modified fiber membrane in a dopamine solution, and controlling the thickness of a polydopamine coating layer by adjusting the concentration of the dopamine solution and the reaction time; carrying out high-temperature carbonization treatment, so as to realize fiber carbonization, and conversion of iron oxide hydroxide to ferroferric oxide as well as polydopamine to a N-doped carbon material; removing ferroferric oxide via soaking in an acid solution. The preparation method is safe and environmentally friendly; the prepared pure carbon fiber material is high in nitrogen content, specific surface area and electric conductivity, and stable in physical and chemical properties, so as to be an ideal electrode material for production of new energy devices such as a supercapacitor.
Owner:FUDAN UNIV

Transportation method for constructing high mountain building

The invention relates to a construction method of a high mountain building, in particular to a transportation method for constructing a high mountain building. In the method, the problems that materials and construction tools are difficult to transport when constructing a new structure or building, and the exiting transportation method has various defects are solved. The method comprises the steps: building a base layer on a slope surface which is relatively flat by the earth excavated on the field; paving two tracks on the base layer; and arranging a transporting hopper car on the tracks, wherein the transporting hopper car is driven by a winding engine at the top of the slope surface to move up and down along the tracks, so that the transportation during constructing the high mountain building is realized. The method is novel and ingenious in design thinking, is reasonable and definite in design parameters, and offers a novel transportation method for the transportation during constructing the high mountain building. The method has the technical effects as follows: 1, the construction cost and the project cost are reduced; 2, the work efficiency is high; 3, the method is convenient and flexible; and 4, the method improves the application, i.e. a beautiful and practical passing steel ladder can be formed only with a little improvement.
Owner:山西太行建设开发有限公司

Synchronous generator and method for constructing mutual feedback system of synchronous motor

The invention relates to a motor linkage technology, in particular to a construction method of mutual feedback system of synchronous generators and synchronous motors, which aims to solve the problems that the existing reducer power-load testing system has high cost and wastes energy. The invention has the following steps: two synchronous motors with the same performance parameters are chosen and then a stator of one motor can rotate relative to a rotor; the two synchronous motors are connected coaxially on the condition that the mechanical phases of the rotors are maintained the same; an electric motor is connected coaxially with the two synchronous motors; the armature outputs of the two synchronous motors are connected through the same phase, and then the angle of one synchronous motor stator is artificially rotated, and the rotated synchronous motor is operated in a state of the generator or the electric motor, while the other synchronous motor is operated in a state of the electric motor or the generator. The testing system constructed with the method is low-cost and energy-saving, and is applicable to the performance testing of reducers, synchronous motors, shafts, torque sensors, electric appliances, cables, and switch devices.
Owner:永济电机天作电气股份有限公司

Method for preparing cobaltous oxide manganese nano flower/carbon sponge flexible composite material

The invention belongs to the field of functionalized porous nano materials, and particularly relates to a method for preparing a cobaltous oxide manganese nano flower / carbon sponge flexible compositematerial. The method comprises the steps of: taking a commercial melamine sponge, then performing washing with distilled water and absolute ethanol, performing drying, and then performing process temperature rise calcining of the melamine sponge under the nitrogen or argon atmosphere to obtain a carbon sponge after cooling; preparing a mixed solution containing a manganese salt and a cobalt salt,immersing the carbon sponge into the mixed solution for the hydrothermal reaction, taking out the carbon sponge after the reaction is finished, washing the carbon sponge with distilled water and performing drying to obtain a manganese-cobalt hydroxide precursor-carbon sponge composite material; and further, performing annealing reaction in the argon atmosphere to obtain a cobaltous oxide manganesenano flower / carbon sponge flexible composite material. The flexible, porous and self-support carbon sponge is taken as a growth template to successfully solve the problem that the nano material is easily gathered, and the obtained composite material has a lot of exposure active sites, abundant pores and good electrical conductivity.
Owner:JIANGSU UNIV

Boron-nitrogen co-doped carbon/manganese oxide composite nanosheet material, preparation method and application

The invention discloses a boron-nitrogen co-doped carbon/manganese oxide composite nanosheet material, a preparation method, and an application of the composite nanosheet material in capacitive deionization or in an electrode material of an electrochemical energy storage device. The preparation method comprises the following steps: adding boric acid into chitosan hydrogel, uniformly mixing the boric acid and the chitosan hydrogel, freeze-drying the mixture, and carbonizing the mixture to obtain boron-nitrogen co-doped carbon nanosheets; and putting the boron-nitrogen co-doped carbon nanosheetsin a potassium permanganate solution for reaction to obtain the boron-nitrogen co-doped carbon/manganese oxide composite nanosheet material. The boron-nitrogen co-doped carbon/manganese oxide composite nanosheet material is of a mutually connected three-dimensional sheet structure. The preparation method provided by the invention is simple and feasible, the reaction conditions are mild, and the carbon nanosheets are of a three-dimensional mutual connection structure. The prepared carbon/manganese oxide composite nanosheet material is rich in nitrogen and boron and is of a mesoporous-dominatedporous structure. The composite nanosheet material shows a good prospect in the fields of preparation of capacitive deionization and super capacitor electrodes and catalyst carriers.
Owner:DONGHUA UNIV

Construction process of mold-free concrete spraying beam

The invention relates to the field of civil engineering construction, and provides a construction process of a mold-free concrete spraying beam. The construction process is used for reinforcing engineering of anchor rod lattice beams in slope protection engineering, foundation pit engineering and the like. The construction process of the mold-free concrete spraying beam comprises the following steps that A, slope treatment is carried out, specifically, a mountain body is excavated in a graded mode according to the designed slope rate, the height of each grade is 8-10m, and the slope surface isleveled or sprayed concrete is adopted for initial protection; B, anchor rod installation (including prestressed anchor rods and non-prestressed full-length bonding anchor rods) is carried out; C, full-length steel bars are arranged along the slope surface in a # shape, a square steel bar cage is formed through binding of stirrups, the sprayed concrete is sprayed back and forth for a plurality oftimes along the steel bar cage in a wet spraying mode to form the lattice beams, and the anchor rods are located at the cross joints of the lattice beams; and D, after the strength of the concrete meets the requirement, the prestressed anchor rods are tensioned and locked, the step A to the step C are repeated to enter the next grade of slope prestressed anchor rod lattice beam construction, andthe construction process is worthy of application and popularization.
Owner:浙江佳途勘测设计有限公司

A kind of synthetic method of 2-iminothiazolidin-4-ketone and its derivatives

InactiveCN102276548AAvoid the tedious process of post-processingFacilitate the cyclization reactionOrganic chemistryThioureaKetone
The invention discloses a method for synthesizing 2-iminothiazolidine-4-one and derivatives thereof. The method comprises the following steps of: reacting water or ethanol serving as a solvent and 1 molar part of thiourea or N,N'-disubstituted thiourea and 1 to 1.5 molar parts of chloroacetic acid which are taken as reaction raw materials at the temperature of between 40 and 100 DEG C for 1 to 10hours; and thus obtaining the 2-iminothiazolidine-4-one or the derivatives thereof after reaction. In the method, the water or the ethanol is taken as the solvent, and the chloroacetic acid is a reaction substrate and also a reaction catalyst; and the acidity of the chloroacetic acid is smartly utilized to self-catalyze the reaction, thiazole heterocycles can be formed through cyclization at higher reaction yield (32.5 to 86.4 percent) under the condition that additional catalysts are not used, and the process that a fussy esterification or amidation reaction is used for derivatization of thechloroacetic acid and the aftertreatment process of waste acid obtained after reaction are avoided. The method for synthesizing the 2-iminothiazolidine-4-one and the derivatives thereof is an environment-friendly synthetic process, is easy to operate, and is particularly suitable for industrialized clean production, and design thought is ingenious.
Owner:XI AN JIAOTONG UNIV

Rivet removing tool and method

The invention provides a rivet removing tool and method. No special tool for removing skew rivets is available at present, rivet heads are removed with a sledge hammer by workers through a self-made tool, then rivet rods are ejected out by means of a sharp tool, the risk is extremely high, and a large number of industrial accidents are caused. A hydraulic station of a field riveting machine is used for supplying power to the rivet removing tool, and the rivet removing tool comprises a removing knife, a fixing sleeve, a positioning sliding block, a movable rivet head, a guide washer, a fixed rivet mold, a fixed rivet head and a spring. The removing knife is clamped in the positioning sliding block and makes contact with a rod of a rivet. The fixed rivet head is fixed to the other end of a rivet clamp. The fixed rivet mold is used for fixing a cap of the rivet. The rod of the rivet is removed out of an inner cavity of the fixed rivet head by applying force through a hydraulic piston rod and then taken out after being clamped. The removing knife is made of a high-strength high-plasticity material and can meet the requirements for hardness and the like, and thus the effect that the rivet removing tool is prevented from being broken in the use process is guaranteed. By the adoption of the rivet removing tool, the effect is quite remarkable, and skew rivets and redundant rivets can be removed rapidly and conveniently.
Owner:SHAANXI HEAVY DUTY AUTOMOBILE
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