The invention relates to the technical field of
ceramic materials, in particular to
vanadium-based
zircon microwave dielectric ceramic and a preparation method thereof.The
vanadium-based
zircon microwave dielectric ceramic is prepared from, by weight, Bi2O3, La2O3, CeO2, Nd2O3, Sm2O3 and NH4VO3, the
chemical formula of the
vanadium-based
zircon microwave dielectric ceramic is (Bi < 0.2 > La < 0.2 > Ce < 0.2 > Nd0. 2Sm < 0.2 >) VO4,
powder of Bi2O3, La2O3, CeO2, Nd2O3, Sm2O3 and NH4VO3 is obtained based on the components of the vanadium-based zircon microwave dielectric ceramic by weight, and original
powder is obtained; stirring and mixing the original
powder, performing
wet grinding treatment and
drying treatment to obtain dried powder, and pre-
sintering the dried powder in the
air atmosphere to obtain pre-sintered powder; a binder is added into the pre-sintered powder for
granulation,
compression molding is carried out,
sintering is carried out in the
air atmosphere, the vanadium-based zircon microwave dielectric ceramic is obtained, the vanadium-based zircon microwave dielectric ceramic has the near-zero resonant frequency
temperature coefficient, the
thermal stability of a device can be guaranteed, and the service life of the device is prolonged. The method is widely used for manufacturing microwave devices such as various dielectric antenna substrates, resonators and filters.