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A kind of anaerobic pipe thread sealant and preparation method thereof

A pipe thread and sealant technology, which is applied in the field of paste sealant and its preparation, can solve the problems of reduced medium resistance, incomplete curing, and reduced sealing performance, and achieves the advantages of easy liquid precipitation, stable performance, and low cost. Effect

Active Publication Date: 2017-10-03
TONSAN ADHESIVES INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This cannot avoid the adverse effects of liquid precipitation on product performance, such as changes in curing speed, incomplete curing, reduced sealing performance, and reduced media resistance, etc.

Method used

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  • A kind of anaerobic pipe thread sealant and preparation method thereof
  • A kind of anaerobic pipe thread sealant and preparation method thereof
  • A kind of anaerobic pipe thread sealant and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 19 parts of polyethylene glycol dimethacrylate oligomer, 22 parts of polyethylene glycol laurate, 1.9 parts of saccharin, 1.5 parts of N, N-dimethylaniline, 0.015 parts of EDTA sodium salt, 0.015 parts of naphthalene Put the quinone into the reaction kettle, and stir it for 1 hour at a speed of 300 rpm until it is completely dissolved. Add 32 parts of bisphenol A fumarate, and stir for 2 hours at 800 rpm until completely dissolved. Then add 7 parts of polytetrafluoroethylene powder, and stir for 30 minutes at a speed of 1000 rpm until the mixture is evenly dispersed. Then add 7 parts of polyethylene powder, 3 parts of titanium dioxide, and 1 part of epoxy resin, and stir for 300 minutes at a speed of 800 to 1000 rpm to disperse evenly. Then add 1.2 parts of cumene hydroperoxide, and stir at a speed of 1000 rpm for 30 minutes until the mixture is uniformly dispersed, and the temperature of the material is controlled below 50° C. during stirring. Add 2.5 parts and the s...

Embodiment 2

[0034] 20 parts of polyethylene glycol dimethacrylate oligomer, 23 parts of polyethylene glycol laurate, 2 parts of saccharin, 1.6 parts of N, N-dimethylaniline, 0.017 parts of EDTA sodium salt, 0.016 parts of naphthalene Put the quinone into the reaction kettle, and stir it for 1 hour at a speed of 300 rpm until it is completely dissolved. Then add 33 parts of bisphenol A fumarate, and stir for 2 hours at a speed of 800 rpm until completely dissolved. Then add 7.5 parts of polytetrafluoroethylene powder, and stir for 30 minutes at a speed of 1000 rpm until the mixture is evenly dispersed. Then add 6.8 parts of polyethylene powder, 2.5 parts of titanium dioxide, and 0.8 parts of epoxy resin, and stir for 300 minutes at a speed of 800 to 1000 rpm to disperse evenly. Then add 1 part of cumene hydroperoxide, and stir at a speed of 1000 rpm for 30 minutes until the mixture is uniformly dispersed, and the temperature of the material is controlled below 50° C. during stirring. Add...

Embodiment 3

[0036] 21 parts of polyethylene glycol dimethacrylate oligomer, 22 parts of polyethylene glycol laurate, 1.8 parts of saccharin, 1.5 parts of N, N-dimethylaniline, 0.015 parts of EDTA sodium salt, 0.01 part of naphthalene Put the quinone into the reaction kettle, and stir it for 1 hour at a speed of 300 rpm until it is completely dissolved. Then add 34 parts of bisphenol A fumarate, and stir for 2 hours at a speed of 800 rpm until completely dissolved. Then add 7 parts of polytetrafluoroethylene powder, and stir for 30 minutes at a speed of 1000 rpm until the mixture is evenly dispersed. Then add 6.2 parts of polyethylene powder, 2.3 parts of titanium dioxide, and 0.9 parts of epoxy resin, and stir for 300 minutes at a speed of 800 to 1000 rpm to disperse evenly. Then add 1 part of cumene hydroperoxide, and stir at a speed of 1000 rpm for 30 minutes until the mixture is uniformly dispersed, and the temperature of the material is controlled below 50° C. during stirring. Add 2...

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Abstract

The invention relates to a paste-like anaerobic pipe thread sealant good in preventing liquid precipitation during storage and a preparation method thereof. It is mainly through the appropriate amount of polyethylene glycol dimethacrylate oligomers, amine accelerators, saccharin, metal chelating agents, stabilizers, plasticizers, heat-resistant enhancers, lubricating fillers, pigments, hydrophilic White carbon black, cationic surfactant and ethanol are prepared by mixing and stirring according to a certain ratio, a certain order of addition and a certain process. The anaerobic pipe thread sealant prepared by the invention has no liquid precipitation and stable performance when stored at room temperature for one year, and has no liquid precipitation when stored at 50° C. for 14 days.

Description

technical field [0001] The invention relates to the field of polymer materials, in particular to a paste sealant and a preparation method thereof. Background technique [0002] Paste anaerobic pipe thread sealant is a kind of anaerobic adhesive, generally composed of (meth)acrylate oligomers, plasticizers, fillers, heat-resistant additives, accelerators, co-accelerators, pigments, Thickener and other components are stirred and dispersed evenly. It is a paste-like liquid-solid mixture before use. When in use, it is applied between the pipe threads, and the pipe threads are screwed together to remove the air between the mating surfaces of the threads. The glue undergoes free radical polymerization and solidifies under the promotion of metal ions. The advantage of paste anaerobic pipe thread sealant is that it has certain viscosity and thixotropy, it is not easy to flow when used, and it has certain self-lubricating and instant sealing properties. [0003] Since the component...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09J171/00C09J171/02C09J123/06C09J127/18C09J11/04C09J11/06C09J11/08C09K3/10
Inventor 韦震宇李印柏林新松翟海潮王兵苏丹杜新宇蔡志伟
Owner TONSAN ADHESIVES INC
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