Ultra-dense concrete polycarboxylate water reducer for nuclear power and preparation method thereof
A water-reducing agent and super-dense technology, applied in the field of ultra-dense concrete polycarboxylate water-reducer for nuclear power and its preparation, can solve the adverse effects of concrete mechanical properties and durability, complex components, polycarboxylate water-reducer Problems such as adsorption-dispersibility and dispersion retention, to achieve the effect of improving self-compacting, improving fluidity, reducing equipment investment costs and energy consumption costs
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Embodiment 1
[0040] A polycarboxylate superplasticizer for nuclear power ultra-dense concrete, comprising the following components and parts by weight per 100 parts:
[0041]Dispersed ether polycarboxylate superplasticizer: 50 parts
[0042] Slump-preserving ether polycarboxylate superplasticizer: 20 parts
[0043] Sodium gluconate: 5 parts
[0044] Polyether modified silicone defoamer: 0.05 parts
[0045] Hydroxypropyl methylcellulose: 2 parts
[0046] Triethanolamine: 1 part
[0047] Sodium nitrite: 0.3 parts
[0048] water: balance
[0049] Among them, the dispersed ether polycarboxylate water reducer is prepared by the following method:
[0050] Add 180 g of TPEG macromonomer and 180 g of water into the reactor equipped with a stirring device at normal temperature, turn on the stirring device, and stir until the TPEG macromonomer is completely dissolved. Add 2.5 g of ammonium persulfate, 1 g of hydrogen peroxide (purity: 35%), and 3.3 g of acrylic acid to the reaction system, an...
Embodiment 2
[0054] A polycarboxylate superplasticizer for nuclear power ultra-dense concrete, comprising the following components and parts by weight per 100 parts:
[0055] Dispersed ether polycarboxylate water reducer: 52 parts
[0056] Slump-preserving ether polycarboxylate superplasticizer: 25 parts
[0057] Sodium gluconate: 3 parts
[0058] Polyether defoamer: 0.01 parts
[0059] Sodium tripolyphosphate: 3 parts
[0060] Triisopropanolamine: 1.5 parts
[0061] Sodium nitrite: 0.2 parts
[0062] water: balance
[0063] Among them, the dispersed ether polycarboxylate water reducer is prepared by the following method:
[0064] Add 180 g of TPEG macromonomer and 230 g of water into the reactor equipped with a stirring device at normal temperature, turn on the stirring device, and stir until the TPEG macromonomer is completely dissolved. Add 4 g of hydrogen peroxide (purity: 35%) and 2.3 g of maleic anhydride to the reaction system, and continue to fully stir the reaction system. ...
Embodiment 3
[0068] A polycarboxylate superplasticizer for nuclear power ultra-dense concrete, comprising the following components and parts by weight per 100 parts:
[0069] Dispersed ether polycarboxylate superplasticizer: 55 parts
[0070] Slump-preserving ether polycarboxylate superplasticizer: 20 parts
[0071] Cane sugar: 5 parts
[0072] Polyether defoamer: 0.05 parts
[0073] Hydroxypropyl methylcellulose: 1 part
[0074] Triisopropanolamine: 1 part
[0075] Methylparaben: 0.2 parts
[0076] water: balance
[0077] Among them, the dispersed ether polycarboxylate water reducer is prepared by the following method:
[0078] Add 180 g of TPEG macromonomer and 200 g of water into the reactor equipped with a stirring device at normal temperature, turn on the stirring device, and stir until the TPEG macromonomer is completely dissolved. Add 2 g of potassium persulfate, 1 g of hydrogen peroxide (purity: 35%), and 2.5 g of maleic anhydride to the reaction system, and continue to full...
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