Oligosaccharide chelated composite trace element mineral matter supplement and preparation method thereof
A compound trace element and mineral supplement technology, applied in animal feed, additional food elements, applications, etc., can solve the problems of complex ingredients, high viscosity, unfavorable production operation and product purification of cane molasses, and achieve improved purity and convenient measurement Accurate, high-purity results
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Embodiment 1
[0035] Take 2.1 moles of sucrose, prepare it into an aqueous solution with a weight concentration of 50%, raise the temperature to 100°C, add sodium hydroxide under stirring until the pH value of the solution remains unchanged at 8.0±0.1, cool down to 50-60°C, and add 0.3 mole of Ferrous sulfate, 0.3 mole of copper sulfate, 0.25 mole of zinc sulfate, 0.1 mole of manganese sulfate and 0.05 mole of cobalt sulfate, heat preservation reaction for 1 hour, add an equal volume of 75% (v / v) alcohol under stirring, precipitate out, filter, and recover the filtrate by distillation Alcohol; the precipitate was put into a box dryer, and dried at 120°C for 30 minutes to obtain a sucrose chelated composite trace element mineral supplement, which was used as a mineral supplement for sows, and 0.5 kg was added per ton of sow feed.
Embodiment 2
[0037] Take 2.3 moles of trehalose, prepare it into an aqueous solution with a weight concentration of 60%, raise the temperature to 105°C, add potassium hydroxide under stirring, until the pH value of the solution remains unchanged at 9.0±0.1, cool down to 50-60°C, and add 0.4 Mole of ferrous sulfate, 0.2 mole of copper sulfate, 0.2 mole of zinc sulfate, 0.1 mole of manganese sulfate and 0.1 mole of cobalt sulfate, heat preservation reaction for 1 hour, add an equal volume of 90% (v / v) alcohol under stirring, precipitate out, filter, and distill the filtrate Recover the alcohol; put the sediment into a box dryer and dry at 120°C for 30 minutes to obtain a trehalose chelated compound trace element mineral supplement, which is used as a mineral supplement for medium and large pigs, adding 1.0 per ton of medium and large pig feed kg.
Embodiment 3
[0039] Take 2.5 moles of raffinose, prepare it into an aqueous solution with a weight concentration of 55%, raise the temperature to 110°C, add potassium hydroxide under stirring until the pH value of the solution remains unchanged at 8.5±0.1, cool down to 50-60°C, and add 0.35 Mole of ferrous sulfate, 0.25 mole of copper sulfate, 0.22 mole of zinc sulfate, 0.1 mole of manganese sulfate and 0.08 mole of cobalt sulfate, heat preservation reaction for 1 hour, add an equal volume of 75% (v / v) alcohol under stirring, precipitate out, filter, and distill the filtrate The alcohol was recovered; the sediment was put into a box dryer, and dried at 120° C. for 30 minutes to obtain a raffinose chelated complex trace element mineral supplement, which was used as a mineral supplement for sows, and 1.0 kg was added per ton of sow feed.
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