A kind of low-viscosity rubber powder modified asphalt and preparation method thereof

A modified asphalt, low-viscosity technology, used in building components, building insulation materials, plastic recycling, etc., can solve the problems of inability to achieve catalytic activation effect, complex activated rubber powder process, affecting low-temperature performance of asphalt, etc. Low temperature performance and storage stability, alleviating black pollution, increasing the effect of high temperature anti-rutting

Active Publication Date: 2021-03-09
TIANJIN HI TECH ENVIRONMENT DEV CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] Patent CN 103468005A discloses a modified low-viscosity rubber asphalt and its preparation method. Rubber powder, base asphalt and polypropylene wax are blended and modified. Polypropylene wax has a lubricating effect, although the viscosity of rubber asphalt can be reduced after adding , but it will greatly affect the low temperature performance of asphalt, resulting in cracking of asphalt pavement at low temperature
[0006] CN 103396669A discloses a microwave desulfurization and cracking waste tire rubber composite modified asphalt and its preparation method. In the method, the waste tire rubber powder and regenerant are treated with microwaves, and then the treated rubber powder is mixed with asphalt and polyethylene wax For blending modification, although the rubber powder has been treated with microwaves, the rubber powder has not been pretreated to make the surface active, so the catalytic activation effect cannot be achieved after microwave treatment, and the rubber powder is simply dried and heated. Although adding polyethylene wax to prepare modified asphalt can reduce the viscosity of rubber asphalt, it will greatly affect the low temperature performance of asphalt, resulting in cracking of asphalt pavement at low temperature
[0007] CN 104559242A discloses a waste rubber powder modified asphalt composition and a preparation method thereof. In the method, the rubber powder is mixed with potassium oleate, sodium dodecylbenzene sulfonate and sodium hydroxide aqueous solution for 60 minutes, and then Dry in an oven at 60°C for about two hours until the activated rubber powder is obtained, and then the activated rubber powder is mixed with asphalt, aromatic oil, polyethylene, etc. to prepare modified asphalt. The process of activated rubber powder prepared by this method is used. Complexity is difficult to achieve in the production process, and the activation effect of this method is poor, and the amount of rubber powder mixed can only reach 6%-20%

Method used

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  • A kind of low-viscosity rubber powder modified asphalt and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Mix 36-mesh waste tire rubber powder, pine tar, tall oil, thiophenol, and aromatic disulfide in a mass ratio of 100:3:2:0.2:0.1, add it to a high-speed mixer for premixing, and stir for premixing The time is 10 minutes, and the rubber powder mixture is prepared; the rubber powder mixture is passed through the conveyor belt and enters the microwave activation processor, the microwave radiation power is 400W, and the radiation time is 1.5min, and the modified rubber powder 1 is obtained through catalytic activation.

[0044] Rapidly heat the base asphalt to 185-190°C, stir and add modified rubber powder 1 which accounts for 25% by mass of the base asphalt, keep warm and pre-mix for 15 minutes in the premixing tank, then grind it through a colloid mill, and then enter The mixing and development tank was kept warm for 3 hours, and finally the cross-linking agent accounting for 0.25% by mass of the base asphalt was slowly added, and the low-viscosity rubber powder modified as...

Embodiment 2

[0046] The base asphalt is rapidly heated to 185-190°C through a heat exchanger, and the modified rubber powder 1 in Example 1, which accounts for 30% by mass of the asphalt, is stirred and added thereto, and is kept warm and premixed for 15 minutes in a premixing tank, and then Grind once with a colloid mill, then enter the stirring development tank for 3 hours of heat preservation and development, and finally slowly add a crosslinking agent accounting for 0.25% of the base asphalt mass percentage, and continue heat preservation and stirring for 1 hour to obtain low-viscosity rubber powder modified asphalt. its performance.

Embodiment 3

[0048] Mix 36-mesh waste tire rubber powder, coal tar, tall oil, rosin, thiophenol zinc salt, and polyalkylphenol sulfide in a mass ratio of 100:2:4:4:0.5:0.5, and add to high-speed mixing Machine for premixing, mixing premixing time is 10 minutes, the rubber powder mixture is obtained; the rubber powder mixture enters the microwave activation processor through the conveyor belt, the microwave radiation power is 600W, the radiation time is 4.0min, and it is obtained through catalytic activation. Modified rubber powder 2.

[0049] Rapidly heat the base asphalt to 185-190°C, stir and add modified rubber powder 2 accounting for 25% by mass of the asphalt, keep warm and pre-mix for 15 minutes in the premixing tank, then grind it through a colloid mill, and then enter the mixing process The development tank was kept warm for 3 hours, and finally the cross-linking agent accounting for 0.3% by mass of the base asphalt was slowly added, and the heat preservation and stirring was conti...

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Abstract

The invention relates to a low-viscosity rubber powder modified asphalt and a preparation method thereof, belonging to the technical field of chemistry. Low-viscosity rubber powder modified asphalt, in parts by weight, includes base asphalt: 100 parts, modified rubber powder: 25-35 parts, crosslinking agent: 0.25-0.5 parts; wherein, the modified rubber powder includes waste Car tire rubber powder: 100 parts, softener: 5‑15 parts, activator: 0.3‑2 parts. The invention reduces the viscosity of the rubber powder modified asphalt, can reduce the difficulty of its production, transportation, mixing and paving, and the paved road surface is easier to compact. The whole process adopts continuous butt joint production, that is, "rubber powder A-rubber powder B-modified asphalt" adopts continuous butt joint, which reduces heat loss and reduces the energy consumption of the whole process.

Description

technical field [0001] The invention relates to a road paving material in the field of highway engineering, in particular to a low-viscosity rubber powder modified asphalt and a preparation method thereof. Background technique [0002] In recent years, the development of domestic road traffic has put forward higher and higher requirements for the performance of asphalt pavement. However, because ordinary asphalt concrete can't solve the contradiction between high-temperature stability and low-temperature crack resistance, many rutting and cracking early failure phenomena appear on asphalt pavement in my country, which seriously affects the efficiency of highway use. At present, it has been widely recognized in the industry to improve the performance of base asphalt by adding polymers, but the high price of styrene-butadiene block copolymer (SBS) results in high cost of modified asphalt materials. Therefore, people have been looking for a A more economical and better perform...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L95/00C08L21/00C08L91/00C08K5/375C08J11/10
CPCC08J11/10C08J2395/00C08J2421/00C08L95/00C08L2201/08C08L2205/03C08L2205/035C08L21/00C08L91/00C08K5/375Y02W30/62
Inventor 李翠红余强王璐
Owner TIANJIN HI TECH ENVIRONMENT DEV CO LTD
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