Hydrogel material for treating heavy metal containing sewage and preparation method of hydrogel material
A hydrogel and heavy metal technology, applied in water/sewage treatment, chemical instruments and methods, adsorption water/sewage treatment, etc., can solve the problem of poor structural stability of hydrogel materials, limited selection of sewage treatment materials, hydrogel materials Few types and other issues, to achieve the effect of high market application prospects, enhanced mechanical properties, and low cost
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Embodiment 1
[0031] A hydrogel material for treating sewage containing heavy metals:
[0032] (1) the sepiolite that is 10 parts by weight and the humic acid that is 3.0 parts by weight are placed in water, and carry out ultrasonic dispersion, form suspension;
[0033] (2) the methacrylic acid that the weight portion is 30, the polyethylene glycol that the weight portion is 20, the polyvinyl alcohol that the weight portion is 5.0, the ammonium persulfate that the weight portion is 0.4, the aluminum sulfate that the weight portion is 0.05 and the weight portion Add 0.05 part of N,N`-methylene acrylamide into the suspension in step (1), and carry out ultrasonic stirring and mixing at a heating temperature of 75°C, with a stirring speed of 400 rpm and a stirring time of 100 minutes, to obtain a homogeneous mixture containing primary products of phytic acid and sepiolite;
[0034] (3) Filter the primary product obtained in step (2) and uniformly mix humic acid and sepiolite, wash the filtered...
Embodiment 2
[0036] A hydrogel material for treating sewage containing heavy metals:
[0037] (1) the sepiolite that is 15 parts by weight and the humic acid that is 5.0 parts by weight are placed in water, and carry out ultrasonic dispersion, form suspension;
[0038] (2) the methacrylic acid that the weight part is 50, the polyethylene glycol that the weight part is 30, the polyvinyl alcohol that the weight part is 7.0, the ammonium persulfate that the weight part is 0.6, the aluminum sulfate that the weight part is 0.10 and weight part Add 0.10 parts of N,N`-methylene acrylamide to the suspension in step (1), and carry out ultrasonic stirring and mixing at a heating temperature of 75°C, with a stirring speed of 400-600rpm and a stirring time of 120 minutes, to obtain a uniform mixture Primary products containing humic acid and sepiolite;
[0039] (3) Filter the primary product obtained in step (2) and uniformly mix humic acid and sepiolite, wash the filtered product with ethanol, and p...
Embodiment 3
[0041] A hydrogel material for treating sewage containing heavy metals:
[0042] (1) the sepiolite that is 12 parts by weight and the humic acid that is 4.2 parts by weight are placed in water, and carry out ultrasonic dispersion, form suspension;
[0043] (2) the methacrylic acid that the weight part is 38, the polyethylene glycol that the weight part is 24, the polyvinyl alcohol that the weight part is 5.9, the ammonium persulfate that the weight part is 0.4, the aluminum sulfate that the weight part is 0.07 and weight part Add 0.08 part of N,N`-methylene acrylamide into the suspension in step (1), and carry out ultrasonic stirring and mixing at a heating temperature of 75°C, with a stirring speed of 480rpm and a stirring time of 100 minutes, to obtain a homogeneous mixture containing primary products of phytic acid and sepiolite;
[0044] (3) Filter the primary product obtained in step (2) and uniformly mix humic acid and sepiolite, wash the filtered product with ethanol, ...
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