Preparation method of brown corundum-ferrosilicon nitride composite material for cement kiln mouth
A technology of ferrosilicon nitride and composite materials, which is applied in the field of advanced refractory materials, and can solve the problems of poor oxidation resistance, unsatisfactory corrosion resistance and low thermal shock resistance of silicon carbide bricks and silicon carbide composite bricks. Problems, achieve good thermal shock stability, excellent corrosion resistance and oxidation resistance, and good thermal shock stability
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example 1
[0016] According to the ratio of raw materials, the mass fraction is 50% brown corundum large particles, 15% brown corundum medium particles, 10% brown corundum fine powder, 5% activated alumina fine powder, 20% ferrosilicon nitride fine powder, and 3 -5% phenolic resin is used as a binder, the raw materials are mixed and then kneaded, and pressed to form under 20MPa. Put the pressed sample into the sintering furnace, pass nitrogen gas with a purity of 0.9999, raise the temperature to 1100°C for 2 hours, carry out nitriding at 1300°C for 8 hours, and then cool naturally to prepare the brown corundum-iron silicon nitride composite refractory material .
example 2
[0018] According to the ratio of raw materials, the mass fraction is 40% brown corundum large particles, 25% brown corundum medium particles, 10% brown corundum fine powder, 20% activated alumina fine powder, 5% ferrosilicon nitride fine powder, and additionally add 3 -5% phenolic resin is used as a binder, the raw materials are mixed and then kneaded, and pressed to form under 20MPa. Put the pressed sample into the sintering furnace, pass nitrogen gas with a purity of 0.9999, raise the temperature to 1100°C for 2h, carry out nitriding at 1500°C for 8h, and then cool naturally to prepare the brown corundum-iron silicon nitride composite refractory material
example 3
[0020] According to the ratio of raw materials, the mass fraction is 40% brown corundum large particles, 25% brown corundum medium particles, 10% brown corundum fine powder, 10% activated alumina fine powder, 15% ferrosilicon nitride fine powder, and 3 -5% phenolic resin is used as a binding agent, the raw materials are mixed and kneaded, and pressed to form under 30MPa. Put the pressed sample into the sintering furnace, pass nitrogen gas with a purity of 0.9999, raise the temperature to 1100°C for 2 hours, carry out nitriding at 1300°C for 8 hours, and then cool naturally to prepare the brown corundum-iron silicon nitride composite refractory material .
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