Firecracker-shaped titanium dioxide/polyimide nano hybrid fiber preparation method
A polyimide and nanofiber technology, applied in the field of fibers, can solve problems such as unfavorable promotion and complexity, and achieve the effects of wide range of use, high photocatalysis and simple preparation process
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[0022] Example 1
[0023] Using pyromellitic anhydride / 4,4'-diaminodiphenylmethane polyamic acid with a solid content of 15%, polyamic acid is obtained by high-voltage electrostatic spinning, and polyimide nanometers are prepared by thermal imide process fiber.
[0024] Put the polyimide nanofibers prepared above into an autoclave containing 0.001g / mL titanium foil and 0.05mol / L hydrochloric acid. Reacted at 170°C for 12 hours to prepare a firecracker-like titanium dioxide / polyimide nano hybrid fiber.
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[0025] Example 2
[0026] Using 3,3',4,4'-biphenyltetracarboxylic dianhydride / 4,4'-diaminodiphenyl ether polyamic acid with a solid content of 20%, the polyamic acid is obtained by high-voltage electrostatic spinning. Polyimide nanofibers are prepared by the imine process.
[0027] Put the polyimide nanofiber prepared above into an autoclave containing 0.002 g / mL titanium powder and 0.1 mol / L hydrochloric acid. The firecracker-like titanium dioxide / polyimide nano-hybrid fiber was prepared by reacting at 150°C for 8 hours.
Example Embodiment
[0028] Example 3
[0029] Using 3,3',4,4'diphenyl ether tetracarboxylic dianhydride / 4,4'-diaminodiphenyl ether polyamic acid with a solid content of 17%, the polyamic acid is obtained by high-voltage electrostatic spinning. Polyimide nanofibers are prepared by the imine process.
[0030] Put the polyimide nanofibers prepared above into an autoclave containing 0.004 g / mL titanium powder and 0.05 mol / L hydrochloric acid. The firecracker-like titanium dioxide / polyimide nano-hybrid fiber was prepared by reacting at 160°C for 10 hours.
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