Bast fiber fabric with protective function and preparation method thereof
A protective function, hemp fabric technology, applied in plant fiber, textiles, papermaking, biochemical fiber treatment, etc., can solve the problems of high harm and single function of functionally modified products, and achieve the promotion of bonding fastness, simple method, and satisfactory ecological effect
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Embodiment 1
[0024] Add ramie fiber to 15wt% sodium hydroxide solution, stir at room temperature for 20 minutes, wash with water 3 times, soak in glacial acetic acid with a mass concentration of 5% for 30 minutes, finally wash with water and dry to obtain alkalized ramie fiber;
[0025] Prepare a sodium periodate solution with a concentration of 2g / L and place it in a brown conical flask, add the alkalized ramie fiber prepared above at a bath ratio of 50:1, and react in a water bath at 40°C for 0.5h to obtain oxidized ramie Fabric: Take out the oxidized ramie fabric and rinse it, soak it in glycerin solution for 2 hours, and then soak it in deionized water for 24 hours. Obtain the oxidized ramie fabric after washing and drying at last;
[0026] The chitosan that weighed deacetylation degree is 80% is added in the dilute acetic acid solution that volume concentration is 1%, and chitosan is dissolved in acetic acid solution completely, wherein the mass concentration of chitosan in the chitos...
Embodiment 2
[0031] Add flax fiber to 25wt% sodium hydroxide solution, stir at room temperature for 60 minutes, wash with water 5 times, soak in glacial acetic acid with a mass concentration of 5% for 30 minutes, finally wash with water and dry to obtain alkalized flax fiber;
[0032] Prepare a periodic acid solution with a concentration of 10g / L and place it in a brown conical flask, add the alkalized flax fiber prepared above at a bath ratio of 50:1, and react in a water bath at 60°C for 3 hours in the dark to obtain oxidized flax fabric; The oxidized linen fabric was taken out and rinsed, then soaked in acetone solution for 2 hours, and then soaked in deionized water for 24 hours. Obtain the oxidized linen fabric after washing and drying at last;
[0033] The degree of deacetylation that weighs is that 95% chitosan joins in the dilute acetic acid solution that volume concentration is 4%, and chitosan is dissolved in acetic acid solution completely, wherein the mass concentration of chit...
Embodiment 3
[0038] The jute fiber is added in 20wt% sodium hydroxide solution, stirred at room temperature for 40min, washed 3 times, then soaked in 5% glacial acetic acid for 30min in mass concentration, finally washed with water and dried to obtain alkalized jute fiber;
[0039] Prepare a sodium periodate solution with a concentration of 8g / L and place it in a brown conical flask, add the alkalized jute fiber prepared above at a bath ratio of 50:1, and react in a water bath at 50°C for 2 hours in the dark to obtain oxidized jute fabric ; The oxidized jute fabric was taken out and rinsed, then soaked in acetone solution for 2 hours, and then soaked in deionized water for 24 hours. Obtain the oxidized jute fabric after washing and drying at last;
[0040] The degree of deacetylation that weighs is that 85% chitosan joins in the dilute acetic acid solution that volume concentration is 1%, and chitosan is dissolved in acetic acid solution completely, wherein the mass concentration of chitos...
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