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Preparation method of size-controllable mono-crystalline zinc oxide nano-rods

A zinc oxide nanorod, single crystal technology, applied in chemical instruments and methods, nanotechnology for materials and surface science, single crystal growth, etc., can solve the problem of poor size controllability of zinc oxide nanorods, easy aggregation, and operation. The process is cumbersome and other problems, to achieve the effect of easy size, good repeatability, and simple operation process

Active Publication Date: 2016-11-16
HENAN NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In summary, the currently reported synthesis method of ZnO nanorods is cumbersome, and the prepared ZnO nanorods have poor size controllability and are easy to agglomerate.

Method used

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  • Preparation method of size-controllable mono-crystalline zinc oxide nano-rods
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  • Preparation method of size-controllable mono-crystalline zinc oxide nano-rods

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Effect test

Embodiment 1

[0017] Dissolve 0.6g of zinc acetate dihydrate in a mixed solution of 3mL of acetic acid and 37mL of diethylene glycol, stir at room temperature until the particles are completely dissolved to obtain a clear solution, transfer the clear solution to a 50mL polytetrafluoroethylene liner, and seal it in The reaction was heated at 150° C. for 6 h in a constant temperature drying oven, and the white precipitate formed by the reaction was washed twice with deionized water and ethanol in turn, and then vacuum-dried at 60° C. to obtain single crystal zinc oxide nanorods ZnO-NR1.

Embodiment 2

[0019] Dissolve 0.8g of zinc acetate dihydrate in a mixed solution of 3mL of acetic acid and 37mL of diethylene glycol, stir at room temperature until the particles are completely dissolved to obtain a clear solution, transfer the clear solution to a 50mL polytetrafluoroethylene liner, seal it in The reaction was heated at 150° C. for 6 hours in a constant temperature drying oven, and the white precipitate formed by the reaction was washed twice with deionized water and ethanol in turn, and then vacuum-dried at 60° C. to obtain single crystal zinc oxide nanorods ZnO-NR2.

Embodiment 3

[0021] Dissolve 1g of zinc acetate dihydrate in a mixed solution of 3mL of acetic acid and 37mL of diethylene glycol, stir at room temperature until the particles are completely dissolved to obtain a clear solution, transfer the clear solution to a 50mL polytetrafluoroethylene liner, seal it and place it at a constant temperature The reaction was heated at 150°C in a drying oven for 6h, and the white precipitate formed by the reaction was washed twice with deionized water and ethanol in turn, and then dried in vacuum at 60°C to obtain single crystal zinc oxide nanorods ZnO-NR3.

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Abstract

The invention discloses a preparation method of size-controllable mono-crystalline zinc oxide nano-rods, and belongs to the technical field of synthesis of nano zinc oxide. The technical solution of the preparation method has the key points of: dissolving zinc acetate dihydrate in a mixed solution of acetic acid and diglycol, performing stirring at room temperature until all particles are dissolved to obtain a clarified solution, transferring the clarified solution into a hydrothermal reaction kettle for reaction at 150 DEG C for 6h, washing white precipitates generated after the reaction with deionized water and ethanol in sequence, and then performing vacuum drying at 60 DEG C to prepare a target product namely the mono-crystalline zinc oxide nano-rods. The preparation method is simple and feasible in operation process, and good in repeatability, the size of the synthesized zinc oxide nano-rods is easy to adjust and control, and the zinc oxide nano-rods can be used for mass production; and the prepared zinc oxide nano-rods are in a mono-crystalline form, and are high in crystallinity and uniform in size, thereby having a relatively good application prospect in the field of photoelectric materials.

Description

technical field [0001] The invention belongs to the technical field of synthesis of nano-zinc oxide, and in particular relates to a method for preparing a size-controllable single-crystal zinc oxide nanorod. Background technique [0002] Zinc oxide is a typical metal semiconductor oxide. It has the characteristics of wide band gap, high exciton binding energy, good thermal stability, simple preparation method, various shapes and sizes, and low price. It can be widely used in ceramics, Chemical, optical, electronic and biological fields. Among them, the one-dimensional zinc oxide nanomaterials have a uniform structure, and most of them are single crystals; they have a high specific surface area; the preferred orientation of crystal growth; fewer crystal defects, which is conducive to the directional transmission of electrons; more obvious quantum size effect, It exhibits unique optical, electrical, and thermal properties, which provide a basis for the development of nanoscal...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C30B29/16C30B7/10B82Y40/00B82Y30/00
CPCB82Y30/00B82Y40/00C30B7/10C30B29/16
Inventor 武大鹏曹锟徐芳高志永马超常玖利蒋凯
Owner HENAN NORMAL UNIV
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