Method for preparing concrete water reducer with styrene sulfonate as monomers
A technology of styrene sulfonate and concrete water reducer, which is applied in the field of preparation of concrete water reducer, can solve the problems of limiting application and improving the effect, and achieve the effect of improving application performance
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[0028] Example 1
[0029] First, 1.43g of methacrylic acid, 10.84g of itaconic acid, 6.19g of sodium p-styrene sulfonate, 14.77g of water, 1.23g of sodium methacrylic acid sulfonate, 21.67g of 10% peroxide were added to the reactor in sequence. Sodium sulfate aqueous solution, and the stirring time is 5 minutes at each feeding interval, and the temperature is raised to 60 ° C to carry out a polymerization reaction, and the reaction is carried out for 6.5 hours to obtain an aqueous solution of polycarboxylic acid-styrene sulfonate; The brine solution was evacuated to remove water in the system, 64.61g of dimethylformamide was added, stirred for 12 minutes, 6.24g of thionyl bromide was added dropwise to the reactor within 0.7 hours under ice-water bath conditions, and the temperature was controlled to react at a constant temperature at 3°C After 17 hours, 123.49 g of methanol was added to wash the precipitate repeatedly for 3 times, and the precipitate was vacuum-dried at 80°C t...
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[0030] Example 2
[0031] After the concrete water reducing agent solution with a mass fraction of 30% obtained in Example 1 was stored at 6° C. for 30 days, its implementation effect was measured.
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[0032] Example 3
[0033] First, 2.87g of methacrylic acid, 4.34g of itaconic acid, 3.87g of maleic acid, 5.15g of sodium p-styrene sulfonate, 16.23g of water, 0.57g of mercaptoacetic acid, 7.13g of 20% mass fraction were added to the reactor in sequence ammonium persulfate aqueous solution, and the stirring time is 11 minutes at each feeding interval, and the temperature is raised to 75 ° C to carry out the polymerization reaction, and the reaction is carried out for 4.5 hours to obtain the polycarboxylic acid-styrene sulfonate aqueous solution; the obtained polycarboxylic acid-styrene The aqueous sulfonate solution was evacuated to remove the water in the system, 40.57g of dimethyl sulfoxide was added, stirred for 14 minutes, and 3.57g of thionyl chloride was added dropwise to the reactor within 0.6 hours under ice-water bath conditions, and the temperature was controlled at a constant temperature of 4°C After 16 hours of reaction, 158.39 g of methanol was added to wash the ...
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