Technology used for recycling copper from copper nitrate waste liquid
A technology for copper nitrate and copper recovery, applied in the field of electrochemical applications, can solve the problems of burning conductive copper rods or electroplating equipment, consuming large energy, nitrogen oxide yellow smoke, etc., avoiding overheating and burning, reducing ammonia nitrogen emissions, and saving material costs Effect
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Embodiment 1
[0022] The present embodiment provides a kind of technique that reclaims copper from copper nitrate waste liquid, and it comprises the steps:
[0023] a, adding molar concentration in copper nitrate waste liquid is the sulfate of 0.01mol / L, the mass ratio of described sulfate and described copper nitrate waste liquid is 1:5, and described sulfate is inorganic sulfate, this implementation In an example, the inorganic sulfate is potassium aluminum sulfate, and when potassium aluminum sulfate is added, stirring is carried out, the stirring speed is 10r / min, and the circulation volume is 10L / min;
[0024] b. Add alkaline neutralizing solution to the solution obtained in step a, adjust the acidity value of the solution to 0.1N, and start electrolysis at a voltage of not less than 12V, and the current density during electrolysis is 180A / m 2 . The alkaline neutralizing solution is an inorganic base. In the present embodiment, the inorganic base is ammonium carbonate with a concentra...
Embodiment 2
[0026] The present embodiment provides a kind of technique that reclaims copper from copper nitrate waste liquid, and it comprises the steps:
[0027] A, adding molar concentration in copper nitrate waste liquid is the sulfate of 0.5mol / L, and the mass ratio of described sulfate and described copper nitrate waste liquid is 1:45, and described sulfate is inorganic sulfate, this implementation In example, described inorganic sulfate is the mixture of potassium sodium sulfate, sodium ammonium sulfate, and wherein, described potassium sodium sulfate accounts for the mass percent of described mixture and is 50%, when adding potassium sodium sulfate, sodium ammonium sulfate, carry out circulation stirring, The stirring speed is 50r / min, and the circulation volume is 250L / min;
[0028] b. Add alkaline neutralizing solution to the solution obtained in step a, adjust the acidity value of the solution to 2.5N, and start electrolysis at a voltage not lower than 12V, and the current densi...
Embodiment 3
[0030] The present embodiment provides a kind of technique that reclaims copper from copper nitrate waste liquid, and it comprises the steps:
[0031] a, adding molar concentration in copper nitrate waste liquid is the sulfate of 0.15mol / L, and the mass ratio of described sulfate and described copper nitrate waste liquid is 1:25, and described sulfate is inorganic sulfate, this implementation In an example, the inorganic sulfate is a mixture of potassium sulfate and magnesium sulfate, wherein the potassium sulfate accounts for 45% by mass of the mixture, and when potassium sulfate and magnesium sulfate are added, the stirring speed is 50 rpm. / min, the circulation volume is 250L / min;
[0032] b. Add alkaline neutralizing solution to the solution obtained in step a, adjust the acidity value of the solution to 1N, and start electrolysis at a voltage not lower than 12V, and the current density during electrolysis is 250A / m 2 . The alkaline neutralizing solution is a mixture of ...
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