Waxberry general flavone preservative solution and application in freshness preservation of aquatic products
A technology of total flavonoids and fresh-keeping liquid, which is applied to the fresh-keeping liquid of red bayberry total flavonoids and its application in the preservation of aquatic products, which can solve the problems that have not been reported, achieve good fresh-keeping effect, prolong shelf life, and delay spoilage and deterioration
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Embodiment 1
[0024] Embodiment 1: preparation of red bayberry total flavonoids fresh-keeping solution
[0025] 1. Extraction process:
[0026] (1) Take fresh bayberry fruit, dry and crush, add 4 times the mass of 95% ethanol to soak for 24 hours, ultrasonically assisted extraction for 45 minutes, repeat the extraction 3 times to obtain the extract, recover the solvent, and concentrate to obtain the extract;
[0027] (2) Disperse the extract in water, extract with petroleum ether, chloroform, and ethyl acetate respectively, take the ethyl acetate extract, dissolve it in water and absorb it through D101 macroporous resin, 15% ethanol, 35% ethanol, 65% ethanol ethanol elution, take 35% ethanol eluent for recovery, and vacuum-dry the eluent to obtain the total flavonoids powder of myrica rubra.
[0028] 2. Determination of total flavonoids in bayberry
[0029] Adopt conventional high-performance liquid chromatography to detect the product gained in the above-mentioned extraction process, and...
Embodiment 2
[0032] Embodiment 2: the fresh-keeping test of aquatic products of total flavonoids fresh-keeping liquid of red bayberry
[0033] 1. Sample processing
[0034] Select a herring with good color and uniform size, cut off the fish head, cut it open from the abdomen, remove the internal organs, cut two pieces of fish meat along the back bone, peel the fish skin, and then cut it into fish fillets with a mass of about 150 grams. After washing with tap water twice, soak in clean water for 10 minutes, remove and drain, and store in the refrigerator to cool down to 4±1°C. Randomly group them into groups, soak them in different concentrations of preservative solutions for 5 minutes at a solid-to-liquid ratio of 15:8, remove and drain, put them into sterile ziplock bags, and store them in a refrigerated 4±1°C to obtain samples from the test group; Soak the green fish in distilled water for 5 minutes, remove and drain, put into a sterile ziplock bag, and refrigerate at 4±1°C to obtain th...
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