Method for detecting solution resorcinol concentration
A technology of resorcinol and quinone, which is applied in the field of detection of resorcinol concentration in solution, can solve the problems of unsatisfactory rapid detection, large consumption of reagents, long analysis time, etc., achieve good thermochemical stability, improve Detection sensitivity, simple preparation effect
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Embodiment 1
[0030] A method for detecting the concentration of resorcinol in a solution, using a three-electrode system to detect the resorcinol in the solution to be tested by cyclic voltammetry, and obtaining the concentration of resorcinol in the solution to be tested according to the linear equation of resorcinol Concentration, the working electrode in the three-electrode system is modified by aminated graphene quantum dots, and the working electrode is a glassy carbon electrode.
[0031] The method for detecting the concentration of resorcinol in the solution, the specific operation of the modification treatment of aminated graphene quantum dots is as follows: the working electrode is immersed in a solution containing 2 mg / mL aminated graphene quantum dots, and taken out after scanning by cyclic voltammetry , dried in an infrared drying oven,
[0032] Among them, the scan parameters are: initial potential 0V, highest potential 1V, lowest point 0V, final potential 0V, scan rate 0.1V / s...
Embodiment 2
[0043] On the basis of embodiment 1, the method for the described detection solution resorcinol concentration, after the working electrode is pretreated, before the aminated graphene quantum dot modification treatment, first undergo the following treatment:
[0044] First prepare an electrolyte containing 10mM zirconium oxychloride and 0.3M potassium chloride with magnetized water, and then immerse the pretreated working electrode in the electrolyte to electrodeposit a layer of nano-zirconia layer; the electrodeposition mentioned here is to use the cycle Voltammetric method deposits 8-10 laps at -1.1V ~ +0.7V and then washes with ultrapure water;
[0045] Grind Phytophthora and propolis into powder respectively and pass through a 200-mesh sieve to obtain Phytophthora powder and propolis powder, mix Phytophthora powder with fumed white carbon black, propolis powder and magnetized water according to the mass ratio of 2:2:1:1000, The dispersion was obtained by ultrasonic dispersi...
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