High-precision compound polishing solution and preparation method thereof
A compound polishing and high-precision technology, applied in the field of ultra-precision polishing, can solve the problems of limited procurement channels of abrasive raw materials, increase the cost of abrasive procurement, etc., and achieve the effects of low cost, high yield and strong continuity
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Embodiment 1
[0032] Silicon oxide (D 10 =2um,D 50 =3um,D 90 =10um), alumina (D 10 =1.8um, D 50 =3um,D 90 =7um) was mixed into grinding agent according to the ratio of 1:1 by mass percentage, and added to the sand mill with deionized water according to the mass ratio of 0.5:1, after stirring evenly, the grinding medium was 0.2mm zirconia ball, 7000r / min Grinding and dispersing at a rotational speed for 2 hours, the particle size distribution of the slurry obtained is D 10 =1.5um, D 50 =2.6um, D 90 =3.5um, add a dispersant made of sodium hexametaphosphate and sodium lauryl sulfate, the amount of dispersant added is 1% of the mass of the abrasive; put the ground and dispersed slurry into a high-speed mixer, and the speed is 800r / min, first add the suspending agent made of hydroxypropyl methylcellulose and xanthan gum at a mass ratio of 1:0.5 according to the mass of the abrasive, and then add borate and mercapto based on 2% of the mass of the abrasive The corrosion inhibitor made of ...
Embodiment 2
[0034] Cerium oxide (D 10 = 0.8um, D 50 = 1um, D 90 =12um), alumina (D 10 =0.6um, D 50 = 1um, D 90 =3um), zirconia (D 10 =0.5um, D 50 = 1um, D 90 =6um) was mixed into an abrasive at a ratio of 1:1:1 by mass percentage, and added to a sand mill with deionized water at a mass ratio of 0.2:1. After stirring evenly, the grinding medium was 0.2mm zirconia balls, Grinding and dispersing at 7500r / min for 3 hours, the particle size distribution of the slurry obtained is D 10 =0.5um, D 50 = 0.8um, D 90=1.2um, add a dispersant made of sodium tripolyphosphate, sodium hexametaphosphate and triethylhexylphosphoric acid, the amount of dispersant added is 2% of the mass of the abrasive; add the ground and dispersed slurry into a high-speed mixer , the rotating speed is 1000r / min, first add the suspending agent made of hydroxyethyl cellulose, xanthan gum and soybean protein glue according to the mass ratio of 1:0.8 according to 3% of the mass of the abrasive, and then add the suspen...
Embodiment 3
[0036] Magnesium oxide (D 10 =0.2um, D 50 =0.5um, D 90 =2um), titanium oxide (D 10 = 0.18um, D 50 =0.5um, D 90 =3um) was mixed into an abrasive at a ratio of 1:1 by mass percentage, and added to a sand mill with deionized water at a mass ratio of 0.6:1. After stirring evenly, the grinding medium was 0.2mm zirconia balls, 8000r / Grinding and dispersing at min speed for 2.5 hours, the particle size distribution of the obtained polishing liquid slurry is D 10 =0.16um, D 50 = 0.3um, D 90 =0.5um, add a dispersant made of sodium pyrophosphate, methyl amyl alcohol and fatty acid polyethylene glycol ester, the amount of dispersant added is 0.5% of the quality of the grinding agent; add the slurry that has been ground and dispersed into a high-speed mixer, The rotating speed is 1000r / min, first add the suspending agent made of methyl cellulose, hydroxypropyl methylcellulose and xanthan gum at a mass ratio of 1:1 according to the mass of the abrasive at 6%, and then add 4% of the...
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