Preparation method and application of pesticide pyraclostrobin supported sample as well as application of pesticide pyraclostrobin supported sample in fluorescent tracing of pathogenic bacteria of asparagus stem blight
A technology for pyraclostrobin and pesticides, which is applied in the field of pesticide loading applications, can solve the problems such as no reports on the application of pesticides being delivered, and achieve the effects of excellent biocompatibility, easy functionalization, and low toxicity functionalization.
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[0041] In order to clearly illustrate the solutions in the present invention, preferred embodiments are given below and detailed descriptions are given in conjunction with the accompanying drawings.
[0042] The preparation method of the sample loaded with pesticide pyraclostrobin in this embodiment comprises the following steps:
[0043] (1) Preparation of carrier material: prepare mesoporous silica carbon quantum dot material as carrier material;
[0044] (1-1) Dissolve cetyltrimethylammonium bromide in water, stir, add sodium hydroxide solution, and heat; when cetyltrimethylammonium bromide is dissolved in water, cetyltrimethylammonium The mass volume ratio of trimethylammonium bromide and water is 0.2:96g / mL; the concentration of sodium hydroxide solution is 2mol / L, and the mass volume ratio of cetyltrimethylammonium bromide and sodium hydroxide solution is 2 / 7g / mL; the mixture was heated to 80°C.
[0045] (1-2) Add ethyl orthosilicate, ethyl acetate and 3-aminopropyltr...
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