Preparation method of high-safety performance lithium-ion battery
A lithium-ion battery and safety performance technology, which is applied in the manufacture of electrolyte batteries, secondary batteries, battery electrodes, etc., can solve the problems of low energy energy density and discontinuity, and achieve high energy density, high mechanical strength, and high temperature resistance. Good results
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Embodiment 1
[0036] A preparation method of a lithium-ion battery with high safety performance, comprising the following steps:
[0037] (1) Preparation of positive electrode sheet:
[0038] Mix and stir zinc acetate and absolute ethanol evenly, then stir in a constant temperature water bath at 40°C for 2 hours to obtain a transparent solution; add triethanolamine to the transparent solution, and continue stirring for 1 hour to obtain a zinc sol; add lithium cobaltate to the zinc sol Continue stirring until the solvent in the sol is completely removed, then dry it at 85°C, and finally put it in a muffle furnace, first raise the temperature to 400°C at a heating rate of 2°C / min, keep the temperature for 30min, and then increase the temperature at 6°C / min The heating rate was raised to 520°C, and the temperature was kept constant for 2 hours. Finally, the temperature was raised to 640°C at a heating rate of 5°C / min, and the temperature was kept constant for 80 minutes. 2+ The molar concentr...
Embodiment 2
[0049] A preparation method of a lithium-ion battery with high safety performance, comprising the following steps:
[0050] (1) Preparation of positive electrode sheet:
[0051] Mix and stir zinc acetate and absolute ethanol evenly, then stir in a constant temperature water bath at 45°C for 1.8 hours to obtain a transparent solution; add triethanolamine to the transparent solution, and continue stirring for 1.5 hours to obtain a zinc sol; add lithium cobaltate to In the zinc sol, continue to stir until the solvent in the sol is completely removed, then dry it at 95°C, and finally place it in a muffle furnace, first raise the temperature to 420°C at a heating rate of 3°C / min, keep the temperature for 25min, and then heat it at 7°C The temperature was raised to 540°C at a heating rate of 5.5°C / min, and the temperature was kept constant for 1.8 hours. Finally, the temperature was raised to 680°C at a heating rate of 5.5°C / min, and the temperature was kept constant for 70 minutes....
Embodiment 3
[0062] A preparation method of a lithium-ion battery with high safety performance, comprising the following steps:
[0063] (1) Preparation of positive electrode sheet:
[0064] Mix and stir zinc acetate and absolute ethanol evenly, then stir in a constant temperature water bath at 50°C for 1.6 hours to obtain a transparent solution; add triethanolamine to the transparent solution, and continue stirring for 2 hours to obtain a zinc sol; add lithium cobaltate to zinc In the sol, continue to stir until the solvent in the sol is completely removed, then dry it at 110°C, and finally place it in a muffle furnace, first raise the temperature to 440°C at a heating rate of 4°C / min, keep the temperature for 20min, and then increase the temperature at 8°C / min. The temperature was raised to 560°C at a heating rate of 1.6 hours, and finally the temperature was raised to 710°C at a heating rate of 6°C / min, and the temperature was kept at a constant temperature for 60 minutes. 2+ The molar...
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