A kind of layer cast graphene-non-metallic composite material and its preparation method
A composite material and non-metallic technology, which is applied in the field of layer casting graphene-non-metallic composite materials and preparation, can solve the problems of easy agglomeration, confinement, high surface activity, etc., and achieve easy processing and use, low resistivity, high The effect of hardness
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Embodiment 1
[0024] The preparation method of the layer-cast graphene-non-metal composite material of this embodiment includes the following steps:
[0025] (1) Under the action of an ultrasonic probe, graphene quantum dots and boron nitride powder are mixed, and the pure water high-pressure liquid flow method is used for high-pressure grinding and shearing. The pressure is 200MPa, the time is 30 minutes, and the temperature is 2°C. Composite slurry material;
[0026] (2) Vacuum drying the prepared composite slurry material at a pressure of 150 Pa and a drying time of 60 minutes to obtain an anhydrous composite powder material;
[0027] (3) The dried anhydrous composite powder material is quenched and refined by laser treatment to promote molecular rearrangement and graft fusion to obtain a layer-casting graphene-non-metal composite material.
[0028] In other embodiments, graphene quantum dots can also be replaced by graphene microplatelets or a mixture of graphene quantum dots and graphene micro...
Embodiment 2
[0030] The preparation method of the layer-cast graphene-non-metal composite material of this embodiment includes the following steps:
[0031] (1) The graphene microchips and carbon fibers are mixed under the action of an ultrasonic reactor, and the composite slurry is prepared by using propanol high-pressure liquid flow method for high-pressure grinding and shearing, the pressure is 200MPa, the time is 30 minutes, and the temperature is 18°C. Body material
[0032] (2) Dry the prepared composite slurry material under normal pressure for a drying time of 10-60 minutes to obtain an anhydrous composite powder material;
[0033] (3) Laser quenching and refining the dried anhydrous composite powder material to promote molecular rearrangement and grafting fusion to obtain a layer-casting graphene-nonmetal composite material.
Embodiment 3
[0035] The preparation method of the layer-cast graphene-non-metal composite material of this embodiment includes the following steps:
[0036] (1) Under the action of an ultrasonic probe, the graphene microchips and the carbon nanotubes are mixed, and a physical grinding method is used for high-pressure grinding and shearing at a pressure of 150 MPa and a time of 45 minutes to prepare a composite slurry material;
[0037] (2) Perform supercritical drying of the prepared composite slurry material with a pressure of 300 Pa and a drying time of 100 minutes to obtain an anhydrous composite powder material;
[0038] (3) Laser quenching and refining the dried anhydrous composite powder material to promote molecular rearrangement and grafting fusion to obtain a layer-casting graphene-nonmetal composite material.
[0039] In other embodiments, the pressure of supercritical drying may be in the range of 10-1000 Pa, and the drying time may be 15-200 min.
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Abstract
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