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Sound-proof material, preparation method and application of sound-proof material

A technology of raw materials and units, applied in the field of sound insulation material preparation, can solve the problems of poor mechanical properties and difficult degradation of 3D printing foam materials, and achieve good sound insulation effect.

Inactive Publication Date: 2017-06-27
广西丰达三维科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The technical problem to be solved by the present invention is to provide a sound-insulating material, a preparation method and its application, so as to solve the problems of refractory degradation and poor mechanical properties of existing 3D printing foam materials

Method used

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  • Sound-proof material, preparation method and application of sound-proof material

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Effect test

preparation example Construction

[0058] The preparation method of described adhesive comprises the following steps:

[0059] (A) preparation concentration is 28-34Be ', and the tapioca starch slurry I that pH value is 3.5-3.9;

[0060] (B) Add dimethyl glutarate, saturated octadecylamide, 2,5-dimethyl-2,5-bis(benzyl) with a concentration of 10%-14% to the tapioca starch slurry I in step A Acyl peroxy)-hexane, vanadium pentoxide, and then carry out cross-linking and grafting reaction at a microwave power of 100-130W, a temperature of 46-52°C, and a stirring speed of 100-160r / min for 1.4-2h to obtain Slurry II;

[0061] (C) Add potassium hydroxide to the slurry II in step B, adjust the pH value to 9.7-10, then add epichlorohydrin and urea, and then stir at a microwave power of 80-100W and a temperature of 62-66°C Carry out the crosslinking reaction for 1-1.5 hours at a rotational speed of 120-180r / min to prepare slurry III;

[0062] (D) adjust the pH value of the slurry III in step C to 8.2-8.4, raise the te...

Embodiment 1

[0074] A sound-insulating material, in parts by weight, made of the following raw materials: 3 parts of graphene, 230 parts of polyethylene, 112 parts of neoprene, 92 parts of polyoxypropylene triol, 28 parts of caprylic triglyceride , 22 parts of methacrylate polymer, 16 parts of brominated paraffin, 15 parts of quartz glass fiber, 10 parts of maleic anhydride, 8 parts of ethylene-ethyl acrylate copolymer, 12 parts of vinyl acetate ethylene copolymer emulsion, triisopropyl 6 parts of alcohol amine, 20 parts of adhesive, 0.5 parts of dispersant, 0.7 parts of tackifier, 1.2 parts of crosslinking agent, 0.8 parts of catalyst, 1 part of plasticizer, 0.8 parts of toughening agent, 0.7 parts of foaming agent, 0.4 parts of foam regulator, 0.3 parts of foam stabilizer, 0.7 parts of curing agent, 2 parts of degradation agent, 0.5 parts of stabilizer;

[0075] The adhesive, in parts by weight, includes the following raw materials: 105 parts of tapioca starch, 6 parts of dimethyl glutar...

Embodiment 2

[0103] A sound-insulating material, in parts by weight, made of the following raw materials: 2.2 parts of graphene, 191 parts of polyethylene, 98 parts of neoprene, 74 parts of polyoxypropylene triol, 22 parts of caprylic triglyceride , 15 parts of methacrylate polymer, 12 parts of brominated paraffin, 10 parts of quartz glass fiber, 8 parts of maleic anhydride, 6 parts of ethylene-ethyl acrylate copolymer, 9 parts of vinyl acetate ethylene copolymer emulsion, triisopropyl 4 parts of alcohol amine, 18 parts of adhesive, 0.4 part of dispersant, 0.5 part of tackifier, 0.9 part of crosslinking agent, 0.6 part of catalyst, 0.8 part of plasticizer, 0.6 part of toughening agent, 0.5 part of foaming agent, 0.3 parts of foam regulator, 0.2 parts of foam stabilizer, 0.6 parts of curing agent, 1.5 parts of degradation agent, 0.3 parts of stabilizer;

[0104] The adhesive, in parts by weight, includes the following raw materials: 46 parts of tapioca starch, 4 parts of dimethyl glutarate,...

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Abstract

The invention discloses a sound-proof material, a preparation method and an application of the sound-proof material. The sound-proof material is prepared from the following raw materials: graphene, polyethene, chloroprene rubber, polyoxypropylene triol, caprylic / capric triglyceride, a methacrylate polymer, brominated paraffin, a quartz glass fiber, maleic anhydride, an ethylene-ethyl acrylate copolymer, acetic acid ethenyl ester copolymer emulsion, trisopropanolamine, an adhesive, a dispersing agent, a tackifier, a cross-linking agent, a catalyst, a plasticizer, a flexibilizer, a foaming agent, a foaming regulator, a foam stabilizer, a curing agent, a degradation agent and a stabilizer. The sound-proof material is prepared by the steps of mixing, extruding and the like. The sound-proof material is applied to 3D (three dimensional) printing. The material is degradable, can be degraded completely after 267-283 days, and a sound reduction index is 25.36-29.51 dB which shows that the material has a good sound-proof effect.

Description

[0001] 【Technical field】 [0002] The invention belongs to the technical field of sound-insulating material preparation, and in particular relates to a sound-insulating material, a preparation method and an application thereof. [0003] 【Background technique】 [0004] Foam material is also called porous material. It is made of resin as the main raw material and has countless micropores inside. It has the functions of light weight, heat insulation, shock resistance and corrosion resistance. It is widely used as packaging materials and car and ship shells. [0005] In 2004, Geim and Novoselov of the University of Manchester in the United Kingdom obtained independent two-dimensional graphene (Gra-phene, GN) crystals by stripping highly oriented graphite through tape, and graphene has become a research hotspot in the field of materials science. one. Graphene is actually a single atomic layer of graphite, which has a unique two-dimensional structure and excellent mechanical, thermo...

Claims

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Application Information

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IPC IPC(8): C08L23/06C08L11/00C08L71/02C08L3/04C08L91/06C08L31/04C08K13/04C08K3/04C08K7/14C08K5/103C08J9/10B33Y70/00C08B31/00
CPCC08L23/06B33Y70/00C08B31/003C08J9/103C08J2203/04C08J2323/06C08J2411/00C08L2201/06C08L2203/14C08L11/00C08L71/02C08L3/04C08L91/06C08L31/04C08K13/04C08K3/04C08K7/14C08K5/103
Inventor 冯可发
Owner 广西丰达三维科技有限公司
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