A kind of preparation method and application of nano flake bismuth oxide
A technology of nanosheets and uses, applied in the field of semiconductor photocatalysts, can solve problems such as the inability to effectively improve the photocatalyst's ability to remove target pollutants, the inability to make good use of visible light, and the complex preparation process of the photocatalyst, so as to achieve enhanced photocatalysis. Performance, low cost, longevity effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] 1. In the first step, add 0.1g of polyaniline into 50mL of nitric acid solution (1mol / L), and stir for 1h;
[0038] 2. In the second step, add 1.5 g of bismuth chloride to the turbid solution obtained in the first step, and stir to dissolve at 50° C.;
[0039] 3. In the third step, add 120 mL of 0.6 mol / L Na dropwise to the turbid solution obtained in the second step 2 CO 3 Solution, after the dropwise addition, the reaction system was aged at 45°C for 24h;
[0040] 4. The fourth step is to centrifuge the product of the third step, wash the obtained precipitate with butanol and ultrapure water three times respectively, and dry at 60°C, put the dried powder in a muffle furnace and roast at 300°C for 1h, that is C / N doped β-Bi available 2 o 3 Nanosheets.
[0041] 5 mg of the resulting C / N doped β-Bi 2 o 3 Nanosheets were added to 10 mL of 3 mg / L EE2 solution. After 30 min in the dark, the photocatalytic degradation was carried out under the irradiation of a 500W x...
Embodiment 2
[0043] 1. In the first step, add 0.1g of polyaniline into 60mL of nitric acid solution (1.5mol / L) and stir for 1h;
[0044] 2. In the second step, add 1 g of bismuth sulfate to the turbid solution obtained in the first step, and stir to dissolve at 60° C.;
[0045] 3. In the third step, add 120 mL of 0.6 mol / L Na dropwise to the turbid solution obtained in the second step 2 CO 3 Solution, after the dropwise addition, the reaction system was aged at 60°C for 7h;
[0046] 4. The fourth step is to centrifuge the product of the third step, wash the obtained precipitate with ethanol and ultrapure water three times respectively, and dry at 60°C, put the dried powder in a muffle furnace and roast at 350°C for 1h, that is C / N doped β-Bi available 2 o 3 Nanosheets.
[0047] 5 mg of the resulting C / N doped β-Bi 2 o 3 Nanosheets were added to 10 mL of 3 mg / L BPA solution. After 30 min in the dark, the photocatalytic degradation was carried out under the irradiation of a 500W xeno...
Embodiment 3
[0049] 1. In the first step, add 0.15g of polyaniline into 70mL of nitric acid solution (1mol / L), and stir for 1h;
[0050] 2. In the second step, add 1.5 g of bismuth nitrate to the turbid solution obtained in the first step, and stir to dissolve at 40°C;
[0051] 3. In the third step, add 160 mL of 0.6 mol / L Na dropwise to the turbid solution obtained in the second step 2 CO 3 Solution, after the dropwise addition, the reaction system was aged at 55°C for 7h;
[0052] 4. The fourth step is to centrifuge the product of the third step, wash the obtained precipitate with DMF and ultrapure water three times respectively, and dry at 60°C, put the dried powder in a muffle furnace and roast at 350°C for 1h, that is C / N doped β-Bi available 2 o 3 Nanosheets.
[0053] 5 mg of the resulting C / N doped β-Bi 2 o 3 Nanosheets were added to 10 mL of 3 mg / L EE2 solution. After 30 min in the dark, the photocatalytic degradation was carried out under the irradiation of a 500W xenon la...
PUM
| Property | Measurement | Unit |
|---|---|---|
| specific surface area | aaaaa | aaaaa |
| thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More