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Preparation method of high-adsorption-capacity water treatment agent

A water treatment agent, high adsorption technology, applied in the direction of adsorption water/sewage treatment, water/sewage treatment, water/sludge/sewage treatment, etc., can solve the problem that the adsorption activity cannot meet the demand, the reuse rate of industrial water is low, and the Water waste and other problems, to achieve excellent adsorption activity, enhanced wear resistance, good acid and alkali resistance

Inactive Publication Date: 2017-08-11
HEFEI LYUJIE ENVIRONMENTAL PROTECTION TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, my country's industrial water consumption is astonishingly wasted. The main reason is that the reuse rate of industrial water is low. Therefore, improving the utilization efficiency of industrial or civil circulating water and adopting environmentally friendly water treatment agents are crucial to saving water resources, reducing production costs and protecting the environment. environment is very important
Due to the high cost of preparation of water treatment agents, the adsorption activity of the heavily polluted fuel industry cannot meet the demand, and it needs to be solved urgently.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A kind of high adsorption capacity water treatment agent preparation method that the present invention proposes, comprises the following steps:

[0019] S1. Soak the corn cob powder in tartaric acid, irradiate with microwaves, and filter to obtain the first prefabricated material;

[0020] S2. Mix vermiculite powder, sodium lauryl sulfate, cocamidopropyl betaine, and water evenly, heat in a water bath, disperse ultrasonically, add succinimide solution, adjust the pH value of the system to 7.1-7.4 with hydrochloric acid, and add Stir the microcrystalline cellulose, suction filter, wash to neutrality, dry, and grind to obtain the second prefabricated material;

[0021] S3. Stir the absolute ethanol and toluene evenly, add the first prefabricated material, the second prefabricated material, and methyltriethoxysilane, heat up and stir, centrifuge, wash with deionized water until the pH value is neutral, dry, and pulverize to obtain Water treatment agent with high adsorptio...

Embodiment 2

[0023] A kind of high adsorption capacity water treatment agent preparation method that the present invention proposes, comprises the following steps:

[0024] S1, send 60 parts of corn cob powder into 120 parts of tartaric acid by weight and soak for 4 days, microwave irradiation treatment for 20min, microwave irradiation power is 1300W, and filter to obtain the first prefabricated material;

[0025] S2. Mix 16 parts of vermiculite powder, 2 parts of sodium lauryl sulfate, 8 parts of cocamidopropyl betaine, and 80 parts of water in parts by weight, heat in a water bath for 20 minutes, the temperature of the water bath is 80 ° C, and ultrasonically disperse for 60 minutes. Add 4 parts of 28wt% succinimide solution, adjust the pH value of the system to 7.1-7.4 with hydrochloric acid, add 4 parts of microcrystalline cellulose and stir for 20 minutes at a stirring speed of 7000r / min, filter with suction, wash until neutral, 75 ℃ drying, grinding to obtain the second preform;

[...

Embodiment 3

[0028] A kind of high adsorption capacity water treatment agent preparation method that the present invention proposes, comprises the following steps:

[0029] S1, send 100 parts of corn cob powder into 100 parts of tartaric acid by weight and soak for 8 days, microwave irradiation treatment for 10 minutes, microwave irradiation power is 1500W, and filter to obtain the first prefabricated material;

[0030] S2. Mix 8 parts of vermiculite powder, 4 parts of sodium lauryl sulfate, 4 parts of cocamidopropyl betaine, and 100 parts of water in parts by weight, heat in a water bath for 10 minutes, the temperature of the water bath is 90 ° C, and ultrasonically disperse for 40 minutes. Add 8 parts of succinimide solution with a concentration of 24 wt%, adjust the pH value of the system to 7.1-7.4 with hydrochloric acid, add 8 parts of microcrystalline cellulose and stir for 10 minutes at a stirring speed of 8000r / min, filter with suction, wash until neutral, 65 ℃ drying, grinding to ...

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Abstract

The invention discloses a preparation method of a high-adsorption-capacity water treatment agent. The preparation method comprises the following steps that corncob powder is fed into tartaric acid for soaking, microwave irradiation treatment is performed, and filtration is performed to obtain a first pre-prepared material; vermiculite power, lauryl sodium sulfate, cocamidopropyl betaine and water are mixed evenly, heating is performed in a water bath, ultrasonic dispersion is performed, a succinimide solution is added, the pH value of a system is regulated with hydrochloric acid to 7.1-7.4, microcrystalline cellulose is added for stirring, suction filtration is performed, washing is performed to reach a neutral state, and drying and grinding are performed to obtain a second pre-prepared material; absolute ethyl alcohol and toluene are evenly stirred, the first pre-prepared material, the second pre-prepared material and methyltriethoxysilane are added, heating and stirring are performed, centrifugation is performed, flushing is performed with deionized water to make pH value neutral, and drying and smashing are performed to obtain the high-adsorption-capacity water treatment agent. The obtained high-adsorption-capacity water treatment agent is large in adsorption capacity and good in hydrophilcity.

Description

technical field [0001] The invention relates to the technical field of water treatment, in particular to a method for preparing a water treatment agent with high adsorption capacity. Background technique [0002] The global shortage of water resources has attracted great attention all over the world. With the continuous development of our country's economy, the environmental burden is also increasing, and the problem of environmental pollution has become an urgent problem to be solved in our country. However, my country's industrial water consumption is astonishingly wasted. The main reason is that the reuse rate of industrial water is low. Therefore, improving the utilization efficiency of industrial or civil circulating water and adopting environmentally friendly water treatment agents are crucial to saving water resources, reducing production costs and protecting the environment. The environment is very important. Due to the high cost of preparation of water treatment ag...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/24B01J20/30C02F1/28
CPCB01J20/20B01J20/22B01J20/24C02F1/283C02F1/285C02F1/286
Inventor 王成刘梅霞潘海洋
Owner HEFEI LYUJIE ENVIRONMENTAL PROTECTION TECH
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