Preparation method of high-adsorption-capacity water treatment agent
A water treatment agent, high adsorption technology, applied in the direction of adsorption water/sewage treatment, water/sewage treatment, water/sludge/sewage treatment, etc., can solve the problem that the adsorption activity cannot meet the demand, the reuse rate of industrial water is low, and the Water waste and other problems, to achieve excellent adsorption activity, enhanced wear resistance, good acid and alkali resistance
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Embodiment 1
[0018] A kind of high adsorption capacity water treatment agent preparation method that the present invention proposes, comprises the following steps:
[0019] S1. Soak the corn cob powder in tartaric acid, irradiate with microwaves, and filter to obtain the first prefabricated material;
[0020] S2. Mix vermiculite powder, sodium lauryl sulfate, cocamidopropyl betaine, and water evenly, heat in a water bath, disperse ultrasonically, add succinimide solution, adjust the pH value of the system to 7.1-7.4 with hydrochloric acid, and add Stir the microcrystalline cellulose, suction filter, wash to neutrality, dry, and grind to obtain the second prefabricated material;
[0021] S3. Stir the absolute ethanol and toluene evenly, add the first prefabricated material, the second prefabricated material, and methyltriethoxysilane, heat up and stir, centrifuge, wash with deionized water until the pH value is neutral, dry, and pulverize to obtain Water treatment agent with high adsorptio...
Embodiment 2
[0023] A kind of high adsorption capacity water treatment agent preparation method that the present invention proposes, comprises the following steps:
[0024] S1, send 60 parts of corn cob powder into 120 parts of tartaric acid by weight and soak for 4 days, microwave irradiation treatment for 20min, microwave irradiation power is 1300W, and filter to obtain the first prefabricated material;
[0025] S2. Mix 16 parts of vermiculite powder, 2 parts of sodium lauryl sulfate, 8 parts of cocamidopropyl betaine, and 80 parts of water in parts by weight, heat in a water bath for 20 minutes, the temperature of the water bath is 80 ° C, and ultrasonically disperse for 60 minutes. Add 4 parts of 28wt% succinimide solution, adjust the pH value of the system to 7.1-7.4 with hydrochloric acid, add 4 parts of microcrystalline cellulose and stir for 20 minutes at a stirring speed of 7000r / min, filter with suction, wash until neutral, 75 ℃ drying, grinding to obtain the second preform;
[...
Embodiment 3
[0028] A kind of high adsorption capacity water treatment agent preparation method that the present invention proposes, comprises the following steps:
[0029] S1, send 100 parts of corn cob powder into 100 parts of tartaric acid by weight and soak for 8 days, microwave irradiation treatment for 10 minutes, microwave irradiation power is 1500W, and filter to obtain the first prefabricated material;
[0030] S2. Mix 8 parts of vermiculite powder, 4 parts of sodium lauryl sulfate, 4 parts of cocamidopropyl betaine, and 100 parts of water in parts by weight, heat in a water bath for 10 minutes, the temperature of the water bath is 90 ° C, and ultrasonically disperse for 40 minutes. Add 8 parts of succinimide solution with a concentration of 24 wt%, adjust the pH value of the system to 7.1-7.4 with hydrochloric acid, add 8 parts of microcrystalline cellulose and stir for 10 minutes at a stirring speed of 8000r / min, filter with suction, wash until neutral, 65 ℃ drying, grinding to ...
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