Ceramic polymer anti-abrasion polypropylene composite material and preparation method thereof

A composite material and polymer technology, which is applied in the field of ceramic polymer wear-resistant polypropylene composite material and its preparation, can solve the problems of poor low-temperature impact performance, easy aging, large molding shrinkage, etc., and achieve excellent wear resistance and mechanical strength , Improve the mechanical strength, improve the effect of wear resistance

Inactive Publication Date: 2017-09-29
周佳瑜
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantages are poor low-temperature impact p

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0018] Example 1

[0019] A ceramic polymer wear-resistant polypropylene composite material, and its preparation method includes the following steps:

[0020] (1) Weigh 30 parts of potassium powder, 63 parts of 1-ethyl-3-methylimidazole ethyl sulfate salt, 4.5 parts of sodium dodecylbenzene sulfonate and 13 parts of methyl methacrylate into the reactor In the medium, the stirring speed is 100r / min, and the system temperature is maintained at 23 ℃ to react 0.5 to obtain modified potassium powder;

[0021] (2) Weigh 35 parts of zinc stearate, 30 parts of calcium stearate, 55 parts of copper stearate, 150 parts of 1-ethyl-3-methylimidazole ethyl sulfate salt and 53 parts of modified potassium powder Add to the reactor at a stirring speed of 73r / min, maintain the system temperature at 22 ℃ and react for 0.4 hours. The product is filtered, dried under vacuum at 80 ℃, -0.06MPa for 0.5 hours, and calcined at 600 ℃ for 3 hours under nitrogen protection. The product was ground, washed with ...

Example Embodiment

[0024] Example 2

[0025] A ceramic polymer wear-resistant polypropylene composite material, and its preparation method includes the following steps:

[0026] (1) Weigh 30 parts of potassium powder, 55 parts of 1-ethyl-3-methylimidazole ethyl sulfate salt, 4 parts of sodium dodecylbenzene sulfonate and 10 parts of methyl methacrylate into the reactor In the medium, the stirring speed is 90r / min, and the system temperature is maintained at 20 ℃ to react 0.5 to obtain modified potassium powder;

[0027] (2) Weigh 35 parts of zinc stearate, 25 parts of calcium stearate, 52 parts of copper stearate, 135 parts of 1-ethyl-3-methylimidazole ethyl sulfate and 45 parts of modified potassium powder Add to the reactor at a stirring speed of 70r / min, maintain the system temperature at 20 ℃ and react for 0.3h. The product is filtered, dried under vacuum at 80℃, -0.06MPa for 0.5h, and calcined at 600℃ for 3h under nitrogen protection. The product was ground, washed with 500mL ethanol for 3 times...

Example Embodiment

[0030] Example 3

[0031] A ceramic polymer wear-resistant polypropylene composite material, and its preparation method includes the following steps:

[0032] (1) Weigh 30 parts of potassium powder, 70 parts of 1-ethyl-3-methylimidazole ethyl sulfate salt, 6 parts of sodium dodecylbenzene sulfonate and 17 parts of methyl methacrylate into the reactor In the medium, the stirring speed is 110r / min, and the reaction temperature is maintained at 26 ℃ for 0.5 to obtain modified potassium powder;

[0033] (2) Weigh 35 parts of zinc stearate, 40 parts of calcium stearate, 65 parts of copper stearate, 170 parts of 1-ethyl-3-methylimidazole ethyl sulfate and 65 parts of modified potassium powder Add to the reactor at a stirring speed of 80r / min and maintain the system temperature at 25 ℃ to react for 1 hour. The product is filtered, dried under vacuum at 80 ℃, -0.06 MPa for 0.5 hours, and calcined at 600 ℃ for 3 hours under nitrogen protection. After grinding, washing with 500mL ethanol for...

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PUM

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Abstract

The invention relates to a ceramic polymer anti-abrasion polypropylene composite material. The ceramic polymer anti-abrasion polypropylene composite material is prepared from the following raw material components: polypropylene, a ceramic polymer, metal alloy powder, polysulfide rubber, epoxy octyl stearate, diisodecyl pentaerythritol diphosphite and zinc stearate, wherein the ceramic polymer is prepared by virtue of the reaction of silicic acid, titanic acid, tungstic acid, molybdic acid, gallic acid, dimethylaminoethyl acrylate, acrylamide and benzoin methyl ether, the metal alloy powder is prepared by virtue of the reaction of zinc stearate, calcium stearate, copper stearate, 1-ethyl-3-methylimidazolium ethylsulfate and modified potassium powder, and the modified potassium powder is prepared by virtue of the reaction of potassium powder, 1-ethyl-3-methylimidazolium ethylsulfate, sodium dodecyl benzene sulfonate and methyl methacrylate. The ceramic polymer anti-abrasion polypropylene composite material has excellent abrasion resistance and mechanical strength.

Description

technical field [0001] The invention relates to a ceramic polymer wear-resistant polypropylene composite material and a preparation method thereof. Background technique [0002] Polypropylene is one of the five general-purpose plastics, which has the advantages of low density, flex resistance, high strength, good insulation, and corrosion resistance. The disadvantages are poor low-temperature impact performance, easy aging, and large molding shrinkage. Polypropylene can be used in various fields such as automobile bumpers, packaging materials, pipes, sheets, rods, and daily necessities. [0003] At present, the wear resistance and mechanical strength of polypropylene materials need to be further improved. The invention uses polypropylene, ceramic polymer, metal alloy powder, polysulfide rubber, and epoxy octyl stearate to prepare ceramic polymer wear-resistant polypropylene composite materials, which are prepared by extrusion, injection molding, molding, blow molding and o...

Claims

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Application Information

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IPC IPC(8): C08L23/12C08L81/04C08L33/14C08K13/06C08K9/10C08K3/08C08K5/1515C08K5/098B29C47/92B29B9/06B29C48/92
CPCC08L23/12B29B9/06B29C48/92B29C2948/92704C08K2003/0825C08K2003/085C08K2003/0893C08L2205/03C08L81/04C08L33/14C08K13/06C08K9/10C08K3/08C08K5/1515C08K5/098
Inventor 周佳瑜
Owner 周佳瑜
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