A kind of preparation method of fruit anthocyanin extract of Aronia nigra
A technology for extracting Aronia nigra and anthocyanin extract, which is applied in the field of medicine and can solve the problems of poor taste, raw fruit taste sour, bad taste and the like
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[0019] In the embodiment of the present invention, a kind of preparation method of the fruit anthocyanin extract of Aronia adenocarpus is provided, comprising the following steps:
[0020] 1) Degreasing the fruit of Aronia nigra;
[0021] 2) then extracted by mixed acid aqueous solution;
[0022] 3) Purifying and extracting the extract from the resin to obtain the dry extract of the fruit of Sorbus nigra.
[0023] Preferably, in one embodiment of the present invention, the degreasing treatment of the Aronia fruit in step 1) is to dry the Aronia fruit naturally so that the water content is lower than 7% by weight, Then reflux degreasing with the petroleum ether (60 ℃ ~ 90 ℃) of liquid material ratio 5:1 (volume:mass ratio), low-temperature drying, make water content be lower than 4% weight, obtain the good Aronia nigra fruit.
[0024] More preferably, in another embodiment of the present invention, the number of reflux degreasing of petroleum ether is 2 times, 30 minutes eac...
Embodiment 1
[0035] Example 1 Preparation of Aronia fruit anthocyanin extract
[0036] 1. Pretreatment of Aronia fruit: Dry the Aronia fruit naturally to make the water content lower than 7%, and then use the oil with a liquid-to-material ratio of 5:1 (volume mL: mass g) Ether (60 ~ 90 ℃) reflux treatment twice, 30min each time, mainly to remove lipids, pigments, etc. Drying at 50°C, so that the water content is lower than 4%, to obtain the pretreated Aronia fruit;
[0037]2. Extraction: the pretreated fruit of Aronia adenocarpus and the mixed acid aqueous solution (the pH value of the mixed acid aqueous solution is 2 to 3, and the mixed acid is a mixture of acetic acid and malic acid in a mass ratio of 1:1) by The liquid-to-material ratio (volume mL:mass g) was mixed at 6:1, soaked in the dark at room temperature for 48 hours, filtered, and the filtrate was set aside, and the filter residue was added to distilled water (according to the above-mentioned Adjust the pH value of the mixed a...
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