Preparation method of polyurethane modified aramid fiber pulp
A technology of polyurethane modification and aramid pulp, which is applied in the direction of spinning solution preparation, conjugated synthetic polymer artificial filament, fiber type, etc., which can solve the problems of high internal rotation resistance, shedding, and poor long-term performance of friction materials and other problems, to achieve the effect of increased surface roughness, no braking low-frequency noise, and excellent braking performance
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[0023] A kind of preparation method of polyurethane modified aramid pulp composite fiber, its preparation process comprises the following steps:
[0024] (1) Under the protection of nitrogen, add 210 parts by weight of N,N-dimethylacetamide and 10 parts of anhydrous calcium chloride to the reactor, raise the temperature to 60°C, and cool down after the calcium chloride is completely dissolved. to room temperature, add 32 parts of p-phenylenediamine and 32 parts of 3,4'-diaminodiphenyl ether, stir and dissolve, then cool the solution to -10°C to -5°C, then add 9 parts of terephthaloyl dichloride vigorously Stir, and after the rod climbing phenomenon occurs, heat up to 80°C, continue to stir for 30 minutes, add calcium hydroxide to neutralize, and obtain a polymer stock solution, dilute with an appropriate amount of N,N-dimethylacetamide solvent, and configure the mass fraction 10-15% aramid spinning solution;
[0025] (2) Preparation of spinning solution:
[0026] Weigh 10 pa...
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