Preparation method of high-toughness refractory material
A refractory, high-toughness technology, applied in the field of refractories, can solve the problems of reducing the service life of refractories, poor mechanical toughness, poor mechanical toughness, etc., to achieve the effect of ensuring fracture toughness, good mechanical properties, and not easy to break
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Embodiment 1
[0033] A method for preparing a high-toughness refractory material, comprising the following steps;
[0034]a) Raw material preparation: prepare raw materials according to the following parts by weight: 100 parts of alumina, 30 parts of magnesium oxide, 2 parts of niobium pentoxide, 1 part of tantalum pentoxide, 2 parts of granulation binder, and 0.5 part of molding binder; The granulation binder is a 5wt% polyvinylidene fluoride N-methylpyrrolidone solution, and the forming binder is a 5wt% polyvinyl alcohol ethanol solution;
[0035] b) Mixing: first dry-mix the alumina and magnesia by ball milling;
[0036] c) Preliminary granulation: spray water into the uniformly mixed alumina and magnesia mixture and vibrate to granulate; the amount of water sprayed is 2wt% of the total weight of alumina and magnesia, and the water spray process is uniformly completed within 10 minutes;
[0037] d) Re-granulation: Add the granulation binder to the primary granulation mixture and ball mi...
Embodiment 2
[0042] A method for preparing a high-toughness refractory material, comprising the following steps;
[0043] a) Raw material preparation: prepare raw materials according to the following parts by weight: 100 parts of alumina, 34 parts of magnesium oxide, 2.7 parts of niobium pentoxide, 1.4 parts of tantalum pentoxide, 2.3 parts of granulation binder, and 0.6 parts of molding binder; The granulation binder is a 5wt% polyvinylidene fluoride N-methylpyrrolidone solution, and the forming binder is a 5wt% polyvinyl alcohol ethanol solution;
[0044] b) Mixing: first dry-mix the alumina and magnesia by ball milling;
[0045] c) Preliminary granulation: Spray water into the uniformly mixed alumina and magnesia mixture and vibrate to granulate; the amount of water sprayed is 4wt% of the total weight of alumina and magnesia, and the water spray process is uniformly completed within 12 minutes;
[0046] d) Re-granulation: Add the granulation binder to the primary granulation mixture an...
Embodiment 3
[0051] A method for preparing a high-toughness refractory material, comprising the following steps;
[0052] a) Raw material preparation: prepare raw materials according to the following parts by weight: 100 parts of alumina, 37 parts of magnesium oxide, 2.4 parts of niobium pentoxide, 1 part of tantalum pentoxide, 2.6 parts of granulation binder, and 0.6 part of molding binder; The granulation binder is a 5wt% polyvinylidene fluoride N-methylpyrrolidone solution, and the forming binder is a 5wt% polyvinyl alcohol ethanol solution;
[0053] b) Mixing: first dry-mix the alumina and magnesia by ball milling;
[0054] c) Preliminary granulation: Spray water into the uniformly mixed alumina and magnesia mixture and vibrate to granulate; the amount of water sprayed is 3wt% of the total weight of alumina and magnesia, and the water spray process is uniformly completed within 10 minutes;
[0055] d) Re-granulation: Add the granulation binder to the primary granulation mixture and dr...
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