Heterogeneous particle-carried inorganic filler and preparation method thereof
A technology of inorganic fillers and inorganic materials, applied in the field of inorganic materials, can solve the problems of sharp rise in dielectric loss, reduced material compressive strength, limited dielectric constant of composite materials, etc., and achieves high dielectric constant and low dielectric loss. Effect
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Embodiment 1
[0024] The preparation method of the inorganic filler loaded with heterogeneous particles in this embodiment comprises the following steps:
[0025] The first step: 1 part of copper gluconate (organic acid metal salt) is dissolved in 10 parts of water to form a solution, and 20 parts of barium titanate spherical particles (inorganic material) with a diameter of 200 nanometers are added and mixed and fully stirred;
[0026] Step 2: After filtering the mixture (without rinsing), put the solid directly into an oven, raise the temperature to 180°C to volatilize the solvent in the mixture, and then keep it warm for 6 hours until copper gluconate thermally cracks on the surface of barium titanate spherical particles , thereby forming barium titanate nanofillers loaded with nanometer copper (20 nanometers).
Embodiment 2
[0028] The preparation method of the inorganic filler loaded with heterogeneous particles in this embodiment comprises the following steps:
[0029] The first step: 1 part of copper gluconate (organic acid metal salt) is dissolved in 10 parts of water to form a solution, and 20 parts of barium titanate spherical particles (inorganic material) with a diameter of 200 nanometers are added and mixed and fully stirred;
[0030] Step 2: After filtering the mixture (without rinsing), put the solid directly into an oven, raise the temperature to 180°C to volatilize the solvent in the mixture, and then keep it warm for 12 hours until copper gluconate thermally cracks on the surface of barium titanate spherical particles , thereby forming barium titanate nanofillers loaded with nanometer copper (about 40 nanometers).
Embodiment 3
[0032] The preparation method of the inorganic filler loaded with heterogeneous particles in this embodiment comprises the following steps:
[0033] Step 1: Dissolve 1 part of zinc gluconate (organic acid metal salt) in 10 parts of boiling water to form a solution, and add 20 parts of barium titanate spherical particles (inorganic material) with a diameter of 200 nanometers to mix and stir well ;
[0034] Step 2: After filtering the mixture (without rinsing), put the solid directly into an oven, raise the temperature to 120°C to volatilize the solvent in the mixture, and then keep it warm for 6 hours until zinc gluconate thermally cracks on the surface of barium titanate spherical particles , thereby forming a barium titanate nanofiller loaded with nanometer zinc oxide (about 20 nanometers).
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