Superconduction magnet fabrication process

A superconducting magnet and manufacturing process technology, applied in the direction of superconducting magnets/coils, insulators, magnetic objects, etc., can solve the problems affecting the safe and reliable operation of the magnet, increasing the time and cost of the magnet, and the low and low temperature thermal conductivity of the insulating layer, etc. Achieve the effect of being conducive to safe and reliable operation, improving low-temperature thermal conductivity and radiation resistance, and simplifying the process

Active Publication Date: 2018-01-05
TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This conventional magnet insulation process undoubtedly increases the time and cost of magnet production, reduces production efficiency, and is not suitable for the production of special magnets
In addition, the insulating layer made of organic resin such as epoxy resin has low low-temperature thermal conductivity and high thermal expansion coefficient, which will generate large thermal stress during the operation of the magnet, which will affect the safe and reliable operation of the magnet. , especially in some large high-field magnets, the problems are more prominent and severe

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Embodiment 1 superconducting magnet insulation manufacturing process

[0023] (1) 100g of liquid polysiloxane and 20g of silicon powder (average particle size 300nm) were mixed uniformly at 35°C by high-speed stirring at a stirring speed of 500rpm, and vacuum degassed at the same time to prepare a mixed solution;

[0024] (2) 125 grams of high-silica glass fiber tapes are immersed in the above-mentioned mixed solution to obtain pre-impregnated high-silica glass fiber tapes;

[0025] (3) Wrap the pre-impregnated high temperature resistant glass fiber tape on the Nb 3 Sn superconducting material (winding thickness 0.2mm), and then wound into a superconducting magnet;

[0026] (4) Place the wound superconducting magnet in an inert gas atmosphere, raise the temperature to 200°C, and keep it for 5 hours, then raise the temperature to 650°C, and keep it for 200 hours to form a dense insulating layer.

[0027] After testing, the interlaminar shear strength of the above-menti...

Embodiment 2

[0028] Embodiment 2 superconducting magnet insulation manufacturing process

[0029] (1) Mix 100g of liquid polysilazane and 20g of aluminum nitride (average particle size: 500nm) at a stirring speed of 800rpm at 40°C with high-speed stirring, and vacuum degassing at the same time to prepare a mixed solution;

[0030] (2) 120 grams of alkali-free aluminosilicate glass fiber fabrics are immersed in the above-mentioned mixed solution to obtain a pre-impregnated high-silica glass fiber tape;

[0031] (3) Wrap the pre-impregnated high-silica glass fiber tape on the Nb 3 Sn superconducting material (winding thickness 0.4mm), and then wound into a superconducting magnet;

[0032] (4) Place the wound superconducting magnet in an inert gas atmosphere, raise the temperature to 150° C., keep the temperature for 5 hours, then raise the temperature to 650° C., and keep the temperature for 200 hours to form a porous insulating layer.

[0033] (5) With 20g of low-viscosity epoxy resin as ...

Embodiment 3

[0035] Embodiment 3 superconducting magnet insulation manufacturing process

[0036] (1) 50g of liquid polysilazane and 7.5g of silicon nitride whiskers (average diameter 100nm, length 5μm) were mixed uniformly at 35°C by high-speed stirring at a stirring speed of 500rpm, and vacuum degassed at the same time to prepare mixed solution;

[0037] (2) 75 grams of high-silica glass fiber tapes are immersed in the above-mentioned mixed solution to obtain pre-impregnated high-silica glass fiber tapes;

[0038] (3) Wrap the pre-impregnated high-silica glass fiber tape on the Nb 3 Al superconducting material (winding thickness 0.1mm), and then wound into a superconducting magnet;

[0039] (4) Place the wound superconducting magnet in an inert gas atmosphere, raise the temperature to 150° C., keep the temperature for 5 hours, then raise the temperature to 850° C., and keep the temperature for 10 hours to form a porous insulating layer.

[0040] (5) With 12g of low-viscosity epoxy res...

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PUM

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Abstract

The invention provides a novel superconduction magnet fabrication process. The novel superconduction magnet fabrication process comprises the steps of (1) mixing a liquid-state polymer and a filler, and performing vacuum degassing to obtain a mixed liquid; (2) immersing a high-temperature resistant glass fiber fabric in the mixed liquid of the step (1); (3) winding the high-temperature resistant glass fiber fabric which is pre-immersed on a superconduction material to form a superconduction magnet; and (4) placing the superconduction magnet of the step (3) in inert gas, rising a temperature to150-250 DEG C, performing heat preservation for 2-5 hours, rising the temperature to 500-1,200 DEG C, and performing heat preservation for 10-450 hours to form a compact or porous ceramic-glass fiberfabric insulation layer. Preferably, the novel superconduction magnet fabrication process also comprises the steps of immersing the insulation layer in low-viscosity epoxy resin, and performing temperature rising and curing to fabricate the superconduction magnet. The insulation process method is simple, the formation of the insulation layer and the thermal treatment of a superconductor are synchronously performed, the insulation process of a superconduction magnet is simplified, the superconduction magnet manufacturing efficiency is improved, and meanwhile, the low-temperature thermal conductivity and the radiation-resistant performance of the insulation layer are improved.

Description

technical field [0001] The invention relates to the technical field of material engineering, in particular to a superconducting magnet insulation manufacturing process. Background technique [0002] Using Nb 3 Sn, Nb 3 When Al and Bi-based high-temperature superconducting materials are used to make high-field superconducting magnets, due to the high brittleness of these superconducting materials, they need to be wound first, and then undergo a long-term high-temperature heat treatment at 650°C or higher. Then, in order to avoid degrading the performance of superconducting materials, it is necessary to carefully wind glass fibers on superconducting materials, and then use organic resins such as epoxy resin as the resin matrix, and resin-pot the superconducting magnets through the vacuum pressure impregnation process. Heating and curing completes the insulation treatment of the magnet. This conventional magnet insulation process undoubtedly increases the time and cost of ma...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F6/00H01F41/02H01B19/00
Inventor 吴智雄张驰黄传军黄荣进李来风
Owner TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI
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