A kind of polyolefin block copolymer hot-melt adhesive and its manufacture method
A technology of polyolefin block and olefin block, which is applied in the field of polyolefin block copolymer hot-melt adhesive and its manufacturing, can solve problems such as complexity and cost increase, achieve excellent adhesive performance, reduce promotion and use, and reduce product cost. cost effect
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[0022]
[0023] The data in the table are all parts by weight.
[0024] The manufacturing methods of the above-mentioned 5 embodiments are as follows: in the first step, the temperature of the reaction kettle is first heated to 202 ℃-220 ℃, and then the chain shuttling polymerization olefin block copolymer and maleic anhydride polybutadiene, peroxide dioxide are added. Cumene (DCP) and antioxidant 1010 were stirred and grafted, and the stirring and grafting time was 10 minutes; in the second step, the temperature of the reactor was reduced to 155°C-160°C, and aldehyde-ketone resin and terpene phenol resin were added. Stir, the melting time is 70 minutes and vacuumize, the degree of vacuum is -0.06mpa~-0.09mpa; in the third step, the outlet of the reactor is connected to the single screw extrusion granulation system for underwater granulation, and then dehydrated, dried and packaged Serve later.
[0025] The test results of the above-mentioned five embodiments are as follow...
Embodiment 1
[0029] Example 1: Chain Shuttle Polymerization The content of the olefin block copolymer is small, the peel strength is small, and the shear strength is poor; the curing time is too long.
Embodiment 2
[0030] Example 2: chain shuttling polymerization The content of the olefin block copolymer is increased, the amount of maleic anhydride polybutadiene is decreased; the peel strength and shear strength are increased, but the technical requirements cannot be met.
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