Flax lignan microencapsulation method
A flax lignan and emulsifier technology, applied in microcapsules, capsule delivery, pharmaceutical formulations, etc., can solve the problems of oxidative degradation, quality degradation, nutritional loss, etc., to improve water solubility, improve compactness, and prolong storage period. Effect
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Embodiment 1
[0023] A microencapsulation method of flax lignans, comprising the following steps:
[0024] (1) Preparation of core material: Dissolve flax lignans in ethanol with a weight ratio of 6 times, then add glycerol monostearate and lecithin emulsifier at a weight ratio of 1:3, flax lignans and emulsifier The weight ratio is 4:1, stir evenly, get core material solution;
[0025] (2) Prepare the wall material: Cyclodextrin, carboxymethyl chitosan octadecyl quaternary ammonium salt and xanthan gum with a weight ratio of 1:0.4:3 are used as the wall material, and 8 times the weight of the wall material is added water, heated up to 55°C, and stirred evenly to obtain wall material suspension;
[0026] (3) Ultrasonic homogenization: Add the above-mentioned core material solution and wall material suspension into an ultrasonic homogenizer at a weight ratio of 1:4, and homogenize for 30 minutes at an ultrasonic power of 200W and a temperature of 50°C to obtain a milky product;
[0027] (4...
Embodiment 2
[0030] A microencapsulation method of flax lignans, comprising the following steps:
[0031] (1) Preparation of core material: Dissolve flax lignans in ethanol with a weight ratio of 8 times, then add glycerol monostearate and lecithin emulsifier at a weight ratio of 1:2, flax lignans and emulsifier The weight ratio is 5:1, stir evenly, get core material solution;
[0032] (2) Prepare the wall material: Cyclodextrin, carboxymethyl chitosan octadecyl quaternary ammonium salt and xanthan gum with a weight ratio of 1:0.2:4 are used as the wall material, and 7 times the weight of the wall material is added water, heated up to 60°C, and stirred evenly to obtain wall material suspension;
[0033] (3) Ultrasonic homogenization: Add the above-mentioned core material solution and wall material suspension into an ultrasonic homogenizer at a weight ratio of 1:5, and homogenize for 25 minutes at an ultrasonic power of 150W and a temperature of 55°C to obtain a milky product;
[0034] (4...
Embodiment 3
[0037] A microencapsulation method of flax lignans, comprising the following steps:
[0038] (1) Preparation of core material: Dissolve flax lignans in ethanol with a weight ratio of 7 times, then add glycerol monostearate and lecithin emulsifier at a weight ratio of 1:4, flax lignans and emulsifiers The weight ratio is 6:1, stir evenly, get core material solution;
[0039] (2) Prepare the wall material: Cyclodextrin, carboxymethyl chitosan octadecyl quaternary ammonium salt and xanthan gum with a weight ratio of 1:0.5:5 are used as the wall material, and 8 times the weight of the wall material is added water, heated up to 50°C, and stirred evenly to obtain wall material suspension;
[0040] (3) Ultrasonic homogenization: Add the above-mentioned core material solution and wall material suspension into an ultrasonic homogenizer at a weight ratio of 1:6, and homogenize for 20 minutes at an ultrasonic power of 250W and a temperature of 60°C to obtain a milky product;
[0041] (...
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Abstract
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