Active carbon regeneration treatment method
A treatment method, activated carbon technology, applied in separation methods, filter regeneration, chemical instruments and methods, etc., can solve the problems of waste of activated carbon resources, low regeneration efficiency, long time for activated carbon regeneration, etc., achieve no loss of specific surface area, improve Effect of regeneration efficiency and reduction of regeneration time
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example 1
[0037] Raw material of waste activated carbon: taken from Shanghai Qingpu District Sewage Treatment Plant.
[0038] A treatment method for activated carbon regeneration, comprising the steps of:
[0039] (1) Take the dry waste activated carbon and add deionized water at a mass ratio of 1:10, place it in an ultrasonic cell pulverizer for 15 minutes at 4°C, 90W, pulse 0.02s, take out the waste activated carbon and rinse it with distilled water to pH 7, filtered, dried at 40°C for 24 hours, crushed through an 80-mesh sieve, and collected the sieved particles to obtain pretreated waste activated carbon powder, which was set aside;
[0040](2) In terms of parts by mass, take 30 parts of pretreated waste activated carbon powder, 18 parts of absolute ethanol, 12 parts of acetylacetone and 30 parts of tetrabutyl titanate and mix evenly to obtain a mixed solution A, calculated by parts by mass, Take 1 part of potassium iodide, 10 parts of acetylacetone, 10 parts of absolute ethanol, a...
example 2
[0044] Raw material of waste activated carbon: taken from Shanghai Qingpu District Sewage Treatment Plant.
[0045] A treatment method for activated carbon regeneration, comprising the steps of:
[0046] (1) Take the dry waste activated carbon and add deionized water at a mass ratio of 1:10, place it in an ultrasonic cell pulverizer, and ultrasonicate for 18 minutes under the conditions of 45°C, 95W, and pulse 0.02s. After taking out the ultrasonic wave, wash the waste activated carbon with distilled water to pH 7.2, filter, dry at 45°C for 24 hours, crush through an 80-mesh sieve, collect the sieved particles, and obtain the pretreated waste activated carbon powder for future use;
[0047] (2) In parts by mass, take 50 parts of pretreated waste activated carbon powder, 25 parts of absolute ethanol, 15 parts of acetylacetone and 40 parts of tetrabutyl titanate and mix them evenly to obtain a mixed solution A. In parts by mass, Take 2 parts of potassium iodide, 15 parts of ace...
example 3
[0051] Raw material of waste activated carbon: taken from Shanghai Qingpu District Sewage Treatment Plant.
[0052] A treatment method for activated carbon regeneration, comprising the steps of:
[0053] (1) Take the dry waste activated carbon and add deionized water at a mass ratio of 1:10, place it in an ultrasonic cell pulverizer, and ultrasonicate for 16.5 minutes under the conditions of 43°C, 93W, and pulse 0.02s. The pH is 7.1, filtered, dried at 43°C for 24 hours, crushed through an 80-mesh sieve, and the sieved particles are collected to obtain pretreated waste activated carbon powder, which is set aside;
[0054] (2) In terms of parts by mass, take 40 parts of pretreated waste activated carbon powder, 16.5 parts of absolute ethanol, 13.5 parts of acetylacetone and 35 parts of tetrabutyl titanate and mix evenly to obtain a mixed solution A, calculated by parts by mass, Take 1.5 parts of potassium iodide, 12.5 parts of acetylacetone, 12.5 parts of absolute ethanol, and...
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