Hyperbranched resin toughening PBT (polybutylece terephthalate) material and preparation method thereof
A hyperbranched resin and toughening technology, which is applied in the field of hyperbranched resin toughened PBT materials and its preparation, can solve the problems that the viscosity change of epoxy resin is difficult to control the curing process, and the packaging efficiency is reduced, so as to improve compatibility and processing performance, improved adhesion, and excellent interfacial adhesion
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[0025] Weighing: 70 kg of PBT, 18 kg of kaolinite, 18 kg of saturated stearylamide, 6 kg of aluminum dihydrogen phosphate, 6 kg of dimethylethanolamine, 7 kg of glass fiber, 6 kg of toughening agent, 2 kg of polyethylene wax , 1682 kg of antioxidants;
[0026] The toughening agent is prepared by mixing the following components in parts by weight: 3.5 parts of hyperbranched resin, 1.5 parts of acrylic acid, and 1 part of acrylic acid copolymer.
[0027] Specific steps are as follows:
[0028] (1), preparation of microcapsule curing agent:
[0029] ①. Under stirring conditions, add 0.5wt% dimethylethanolamine aqueous solution and 0.5wt% aluminum dihydrogen phosphate aqueous solution, and disperse for 40 minutes under mechanical stirring at 800 rpm to obtain an aqueous phase;
[0030] 2. In the dichloromethane solvent, add kaolinite and saturated stearylamide, and disperse evenly in an ultrasonic instrument to obtain an oil phase, and gradually add the water phase prepared in s...
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