Preparation method for durable anti-bacterial fabric

An antibacterial fabric, durable technology, applied in the direction of plant fiber, animal fiber, textile and paper making, etc., to achieve the effect of obvious antibacterial effect, less damage to the original performance of the fabric, and simple processing technology

Active Publication Date: 2018-03-20
DONGHUA UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in recent years, research results have shown that nano-sized heavy metals and compounds and antibacterial polymer nanoparticles have more excellent antibacterial activity, which is due to the unique nano-effects of nano-sized materials, but this nano-sized antibacterial However, reports on the application of agents to textile materials are limited to inorganic metals and their metal compound nanoparticles.
There are few reports on the successful cases of antibacterial polymer nanoparticles applied to textile materials

Method used

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  • Preparation method for durable anti-bacterial fabric
  • Preparation method for durable anti-bacterial fabric
  • Preparation method for durable anti-bacterial fabric

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] (1) Dissolve 5 g of polyhexamethylene guanidine hydrochloride in 25 mL of deionized water, add 3.5 mL of triethylamine, stir to mix the solution well, then add 8 mL of dioxane solution containing 4 g of methacrylic anhydride dropwise , continue to react for 8h, the product is precipitated with acetone and then dried in a vacuum oven at room temperature to obtain the antibacterial monomer.

[0039](2) In a 250mL three-necked flask, 5g of the antibacterial monomer in step (1), 1.8g of methyl methacrylate and 0.2g of hydroxyethyl methacrylate were dissolved in 100mL of deionized water, and 0.1g of N,N- For methylene bisacrylamide, heat up to 70°C with nitrogen gas for 30 minutes, add 2 mL of an aqueous solution containing 70 mg ammonium persulfate APS dropwise, and continue the reaction for 12 hours. The reaction product is filtered and purified three times, and dried in a vacuum oven at 40°C. antibacterial nanohydrogels.

[0040] (3) Dissolve 0.3 g of the antibacterial n...

Embodiment 2

[0047] (1) Dissolve 5 g of polyhexamethylene guanidine hydrochloride in 25 mL of deionized water, add 3.5 mL of triethylamine, stir to mix the solution well, then add 8 mL of dioxane solution containing 4 g of methacrylic anhydride dropwise , continue to react for 8h, the product is precipitated with acetone and then dried in a vacuum oven at room temperature to obtain the antibacterial monomer.

[0048] (2) In a 250mL three-necked flask, dissolve 8g of the antibacterial monomer in step (1), 1.8g of styrene and 0.2g of hydroxyethyl methacrylate in 100mL of deionized water, and add 0.1g of N,N-methylene For bisacrylamide, heat up to 70°C with nitrogen gas for 30 minutes, add 2 mL of an aqueous solution containing 70 mg of ammonium persulfate APS dropwise, and continue the reaction for 12 hours. The reaction product is filtered and purified three times, and dried in a vacuum oven at 40°C to obtain antibacterial nanoparticles Hydrogels.

[0049] (3) Dissolve 0.3 g of the antibac...

Embodiment 3

[0053] (1) Dissolve 5g of L-arginine in 25mL of deionized water, and add 3.5mL of triethylamine, stir to mix the solution well, then add 8mL of dioxane solution containing 4g of methacrylic anhydride dropwise, continuously After reacting for 8 hours, the product was precipitated with acetone and then dried in a vacuum oven at room temperature to obtain the antibacterial monomer.

[0054] (2) In a 250mL three-necked flask, dissolve 5g of the antibacterial monomer in step (1), 1.8g of styrene and 0.2g of hydroxyethyl methacrylate in 100mL of deionized water, and add 0.1g of N,N-methylene For bisacrylamide, heat up to 70°C with nitrogen gas for 30 minutes, add 2 mL of an aqueous solution containing 70 mg of ammonium persulfate APS dropwise, and continue the reaction for 12 hours. glue.

[0055] (3) Dissolve 0.3g of the antibacterial nano-hydrogel in step (2) in 100mL petroleum ether, ultrasonically disperse for 30min, add 2mL isophorone diisocyanate dropwise, add 0.1mL dibutylti...

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Abstract

The invention relates to a preparation method for durable anti-bacterial fabric. The preparation method comprises the following steps of synthesis of anti-bacteria monomer, synthesis of anti-bacterialNano-hydrogel, synthesis of surface-modified anti-bacterial Nano-hydrogel, and synthesis of durable anti-bacterial fabric. By adopting the preparation method, the anti-bacterial function of the fabric is achieved by combining Nano-hydrogel particles and the fabric. The treatment process of the method is easy and convenient, is low in damage on the original performance of the fabric; the fabric treated with the method has a durable anti-bacterial effect; the prepared anti-bacterial Nano-hydrogel has a simple treatment process, high biocompatibility, remarkable anti-bacterial effect, no injuryon human bodies, no antibacterial agent, and bacterial resistance.

Description

technical field [0001] The invention belongs to the field of preparation of modified textiles, in particular to a preparation method of durable antibacterial fabrics. Background technique [0002] In recent years, with the continuous emergence of new pathogens, the impact of microbial contamination and disease spread caused by bacterial pathogens on human health and life has become more and more serious, and antibacterial research is urgent. [0003] Generally speaking, the surface of materials provides a good medium for the growth of various bacterial pathogens, and the proliferation of bacterial pathogens will have various adverse effects on human safety. Survey data show that after antibacterial treatment on the surface of materials, the probability of microbial contamination and infection will be significantly reduced. Therefore, it is very necessary for the materials used in our daily life to undergo antibacterial modification treatment, so that people's healthy life c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/564C08G18/62D06M101/10D06M101/06
CPCC08G18/6216C08G18/6225D06M15/564D06M16/00D06M2101/06D06M2101/10
Inventor 吴德群韩华覃小红李发学王学利俞建勇石松吴育雷唐萍
Owner DONGHUA UNIV
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