Composite raw material for preparing polyamide film and preparation method of composite raw material
A polyamide film and polyamide technology, which is applied in the field of polyamide film preparation, can solve the problems of insignificant improvement of finished film properties, defects in film products, easy agglomeration of inorganic powders, etc., achieving good opening and preventing agglomeration or precipitation. , the effect of improving compatibility
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Embodiment 1
[0032] 2.5 parts of silicon dioxide with an average particle size of 0.5 microns and 3 microns each, surface-treated with a silane coupling agent, and 100 parts of molten caprolactam monomer under the action of a high-shear disperser to prepare an additive mother liquor.
[0033] 100 parts of caprolactam monomer, 2 parts of desalted water, and 3 parts of additive mother liquor are mixed by a static mixer, and then continuously enter into a two-stage polymerization reactor. The pressure of the front polymerization tube is 0.15MPa, and the reaction temperature is 260-270°C; the pressure of the rear polymerization tube is -0.03MPa, and the reaction temperature is 250-260°C. Polyamide 6 obtained through polymerization was granulated, extracted and dried, and mixed with 0.05% ethylene bisstearamide in a conical double-helix mixer for 20 minutes to obtain polyamide product A for membranes.
Embodiment 2
[0035] The polymerization process was the same as in Example 1, except that the inorganic additives were changed to talcum powder with an average particle size of 0.8 microns and calcium carbonate with an average particle size of 2 microns to obtain polyamide product B for membranes.
Embodiment 3
[0037] The polymerization process was the same as in Example 1, changing 100 parts of caprolactam monomers to 80 parts of caprolactam monomers, and 40 parts of 50% nylon 66 saline solution. Obtain polyamide product C for film
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