A kind of preparation method of nano-ceramic bond
A vitrified bond and nanotechnology, which is applied in the manufacture of tools, clay products, metal processing equipment, etc., can solve the problems of low strength of vitrified bond, poor fatigue resistance, high sintering temperature, etc., and achieve short reaction time and high bending strength The effect of large and low reaction temperature
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Embodiment 1
[0026] A preparation method of nano vitrified bond, said preparation method comprises the following steps:
[0027] a, take by weighing 44g talc, 11g kaolin, 22g boron glass, 8.8g fluorite and 24.2g quartz powder respectively, cross 200 mesh sieves after grinding, and make the mixture;
[0028] b. After briquetting the mixture prepared in step a with a mold, raise the temperature up to 400°C at a rate of 10°C / min, then raise it to 1400°C at a rate of 5°C / min, and keep it warm for 8 hours. The glass frit flowing down after melting is water quenched;
[0029] c. Dry the product obtained in step b at 80°C for 16 hours, add 1.1g of nano vanadium nitride / chromium nitride composite powder (the mass ratio of vanadium nitride to chromium nitride is 1:1), grind, and pass through 200 Mesh sieve to obtain basic vitrified bond;
[0030] d. The basic vitrified bond prepared in step c is pressed into a blank by a press, and sintered in a microwave sintering furnace (sintering temperature ...
Embodiment 2
[0033] A preparation method of nano vitrified bond, said preparation method comprises the following steps:
[0034] a, take by weighing 36.5g talcum, 18.5g kaolin, 15.4g boron glass, 8.4g fluorite and 21.2g of quartz powder respectively, pass through a 200 mesh sieve after grinding to prepare the mixture;
[0035] b. After briquetting the mixture prepared in step a with a mold, raise the temperature up to 400°C at a rate of 5°C / min, then increase to 1200°C at a rate of 2°C / min, and keep it warm for 4 hours. The glass frit flowing down after melting is water quenched;
[0036] c. Dry the product obtained in step b at 120°C for 10 hours, then add 1.5g of nano-vanadium nitride / chromium nitride composite powder (the mass ratio of vanadium nitride to chromium nitride is 1:1), grind and pass 300 mesh sieves were used to obtain the basic vitrified bond;
[0037] d. The basic vitrified bond prepared in step c is pressed into a blank by a press, and sintered in a microwave sintering ...
Embodiment 3
[0040] A preparation method of nano vitrified bond, said preparation method comprises the following steps:
[0041] a, take by weighing 66.5g talcum, 26.25g kaolin, 29.75g boron glass, 14g fluorite and 38.5g quartz powder respectively, cross 200 mesh sieves after grinding, and make the mixture;
[0042] b. After briquetting the mixture prepared in step a with a mold, raise the temperature to 400°C at a rate of 8°C / min, then increase to 1350°C at a rate of 4°C / min, and keep it warm for 6 hours. The glass frit flowing down after melting is water quenched;
[0043] c. Dry the product obtained in step b at 100°C for 12 hours, then add 1.25g of nano-vanadium nitride / chromium nitride composite powder (the mass ratio of vanadium nitride to chromium nitride is 1:1), grind and pass 200 mesh sieves, obtained basic vitrified bond;
[0044] d. The basic vitrified bond prepared in step c is pressed into a blank by a press, and sintered in a microwave sintering furnace (sintering temperat...
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