A kind of preparation method of textile smoothing agent

A technology of smoothing agent and emulsifier, applied in the field of preparation of textile smoothing agent, can solve the problems of general application effect, easy stratification, poor emulsion stability, etc., and achieve the effect of solving easy demulsification, eliminating oil slick and improving stability.

Active Publication Date: 2020-06-30
浙江凯洛琪服饰有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a preparation method of a textile smoothing agent in view of the fact that most of the smoothing agents on the market are organosilicon softening and smoothing agents, the application effect is general, and there are problems of easy delamination and poor emulsion stability

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0020] A kind of preparation method of textile smoothing agent, this preparation method comprises the steps:

[0021] (1) In parts by weight, take 10-15 parts of octamethylcyclotetrasiloxane, 5-6 parts of epichlorohydrin, 2-3 parts of anhydrous tin tetrachloride, and 1-2 parts of sodium hydroxide , mix octamethylcyclotetrasiloxane, epichlorohydrin, and anhydrous tin tetrachloride, heat up to 70~80°C, keep warm for 5~6h, wait until the temperature drops to 50~60°C, add sodium hydroxide Mix and let it stand for 4~5h, then carry out vacuum distillation under the conditions of vacuum degree 13.3Pa and temperature 55~65℃ to obtain distillate, according to the mass ratio of 3~4:5~6:7~8, distillate , toluene, and sodium hydroxide solution were mixed, left to stand for 1-2 hours, and then subjected to vacuum distillation at a vacuum degree of 13.3 Pa and a temperature of 55-65°C to obtain a distillate;

[0022] (2) In parts by weight, take 10-15 parts of organic amine, 7-8 parts of p...

Embodiment 1

[0026] The organic amine is hexamethylenediamine.

[0027] The emulsifier is obtained by mixing dodecylbenzenesulfonic acid and sorbitan monolaurate evenly at a mass ratio of 1:1.

[0028] The catalyst is hydrochloric acid.

[0029] A kind of preparation method of textile smoothing agent, this preparation method comprises the steps:

[0030] (1) In parts by weight, take 10 parts of octamethylcyclotetrasiloxane, 5 parts of epichlorohydrin, 2 parts of anhydrous tin tetrachloride, and 1 part of sodium hydroxide, and mix octamethylcyclotetrasiloxane with Mix oxane, epichlorohydrin, and anhydrous tin tetrachloride, heat up to 70°C, keep warm for 5h, wait until the temperature drops to 50°C, add sodium hydroxide to mix, let stand for 4h, and then vacuum at 13.3Pa, Under reduced pressure distillation at a temperature of 55°C, the distillate was obtained, and the distillate, toluene, and sodium hydroxide solution were mixed according to a mass ratio of 3:5:7, and left to stand for 1...

Embodiment 2

[0035] The organic amine is N,N-diethylpropylenediamine.

[0036] The emulsifier is obtained by mixing dodecylbenzenesulfonic acid and sorbitan monolaurate evenly at a mass ratio of 1:1.

[0037] The catalyst is hydrochloric acid.

[0038] A kind of preparation method of textile smoothing agent, this preparation method comprises the steps:

[0039] (1) In parts by weight, take 15 parts of octamethylcyclotetrasiloxane, 6 parts of epichlorohydrin, 3 parts of anhydrous tin tetrachloride, and 2 parts of sodium hydroxide, and mix octamethylcyclotetrasiloxane with Mix oxane, epichlorohydrin, and anhydrous tin tetrachloride, heat up to 80°C, keep warm for 6h, wait for the temperature to drop to 60°C, add sodium hydroxide to mix, let stand for 5h, and then vacuum at 13.3Pa, Under reduced pressure distillation at a temperature of 65°C, the distillate was obtained. The distillate, toluene, and sodium hydroxide solution were mixed according to a mass ratio of 4:6:8, and left to stand f...

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PUM

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Abstract

The invention discloses a preparation method of a textile smoothing agent, and belongs to the field of textile additives. Polydimethylsiloxane is added for sursurface graft modification of nano silica, the sursurface-graft-modified nano silica is added into emulsion, since the sursurface of the nano silica is coated with the polydimethylsiloxane in the form of a silicon-oxygen bond, organic components on the sursurface of particles are increased, the content of hydroxyl groups on the sursurface is reduced, electronegativity is reduced, hydrophobic properties are improved, defoaming and antifoaming properties are better, and the problems of emulsification difficulty and easy delamination of organosilicone can be better solved. The preparation method solves the problem that smoothing agentson the market in the prior art mostly belong to organosilicone softening smoothing agents, have a general application effect, and have the problems of easy delamination and poor emulsion stability.

Description

technical field [0001] The invention belongs to the field of textile additives, and in particular relates to a preparation method of a textile smoothing agent. Background technique [0002] Smoothing agent is a textile additive used in the textile industry. In the textile printing and dyeing industry, smoothing agent can give plush fabrics, leather fabrics, and cotton fabrics a smooth feel, and can make textiles soft, smooth and bright. It is suitable for the finished products of various fibers. It has excellent gloss, resistance to dry and wet rubbing, flexibility, strong adhesion, waterproof and anti-fouling, fast drying, high and low temperature resistance, and smooth and delicate hand feeling. Some smoothing agents are solid With high content and good dispersibility, it can be diluted with water in any proportion, thus effectively prolonging the shelf life. The smoothing agent can improve the gloss of the fabric and endow the fabric with good smoothness and gloss, so it...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M15/647D06M11/79D06M13/256D06M15/09C08G77/46
CPCC08G77/46D06M11/79D06M13/256D06M15/09D06M15/647D06M2200/50
Inventor 董晓乔舍程依
Owner 浙江凯洛琪服饰有限公司
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