Micro-nano structure array heat dissipation surface and preparation method thereof
A technology of heat dissipation surface and micro-nano structure, applied in the fields of nanotechnology, nanotechnology, nanotechnology, etc. for materials and surface science, can solve the problems of deterioration, phase transformation heat can not strengthen, poor wettability, etc. , to achieve the effect of delaying drying, easy large-scale preparation and low cost
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[0027] At the same time, the present invention also proposes a preparation method for preparing a micro-nano structure array heat dissipation surface, which is characterized in that it comprises the following steps: 1) adding 20-80 parts by weight of fluorine-containing polymer emulsion, 20-80 parts by weight of Heat conductive particles, 5-20 parts by weight of solvent, 0.5-5 parts by weight of additives, etc. are stirred and mixed evenly to obtain a slurry; 2) The slurry prepared in step 1) is printed on the surface of the heat dissipation substrate by screen printing technology, Drying to remove the solvent, and then heat treatment in a protective atmosphere, so that the fluorine-containing polymer resin is cured on the surface of the heat dissipation matrix, thereby obtaining a heat dissipation surface with a micro-nano structure array.
[0028]The fluorine-containing polymer emulsion is one of polytetrafluoroethylene emulsion and polyvinylidene fluoride emulsion; the heat-...
Embodiment 1
[0033] Stir and mix 20g polytetrafluoroethylene emulsion, 30g aluminum powder with a particle size of 1-10 microns, 50g alumina powder with a particle size of 0.1-2 microns, 5g distilled water, 4.5g dispersant, 0.4g wetting agent, 0.1 defoamer, etc. Obtain the printing paste evenly; use a 20-mesh printing screen with a screen size of 250 microns, print the prepared paste on the surface of a clean heat-dissipating aluminum material, dry it in an oven for 2 hours to remove the solvent; then transfer to a nitrogen atmosphere to protect the heating furnace , heat treatment at 250°C for 0.5-1h, to solidify polytetrafluoroethylene and heat-conducting particles on the surface of the heat-dissipating aluminum material, thereby obtaining a heat-dissipating surface with a micro-nano structure array.
[0034] In the obtained micro-nano structure array, the height of the polytetrafluoroethylene / heat-conducting particle composite cone is 200-250 microns, the central moment between the cones...
Embodiment 2
[0036] Stir and mix 80g of polyvinylidene fluoride emulsion, 5g of silver powder with a particle size of 0.5 to 3 microns, 15g of aluminum nitride powder with a particle size of 0.1 to 1 micron, 20g of ethylene glycol, 0.3g of a dispersant, and 0.2g of a thickener to obtain a printed product. Slurry; 400 mesh printing screens with 25 microns of mesh are used to print the prepared slurry on the surface of a clean heat-dissipating copper material, and dry in an oven for 1h to remove the solvent; then transfer to an argon atmosphere to protect the heating furnace, Heat treatment at 150°C for 1 hour to solidify the polyvinylidene fluoride and heat-conducting particles on the surface of the heat-dissipating copper material, thereby obtaining a heat-dissipating surface with a micro-nano structure array.
[0037] In the obtained micro-nano structure array, the height of the polyvinylidene fluoride / heat-conducting particle composite cone is 5-25 microns, the central moment between the ...
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