Method for anion anti-mite antibacterial fiber film for carpet
An antibacterial fiber and negative ion technology, which is applied in fiber processing, fiber chemical characteristics, rayon manufacturing and other directions, can solve the problems of poor antibacterial durability, complex preparation process and high production cost, and achieve strong antibacterial ability, simple preparation method and production process. Efficient effect
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[0028] A kind of preparation method of negative ion anti-mite antibacterial fiber film for carpet, described method is carried out according to the following steps:
[0029] The preparation of step A spinning dope
[0030] According to the following mass percentage:
[0031] Chitosan 8-18%
[0032] Organic solvent 76-90%
[0033] Active mineral powder 2-13%
[0034] Let the weight average molecular weight be M w =80000~200000g / mol chitosan is added to the organic solvent, mechanically stirred for 90 minutes and then dissolved, then the active mineral powder is added, and the spinning solution is obtained after ultrasonic dispersion at a temperature of 10~45°C for 2~5 hours. The organic solvent is N,N-dimethylformamide or 3%-60% acetic acid aqueous solution or one of dioxane or peracetic acid, and the active mineral powder is tourmaline, diatomaceous earth, Medical stone and titanium dioxide are mixed, and its mass ratio is 3:2:3:2, and tourmaline is a mixture of magnesiu...
Embodiment 1
[0040]Add chitosan with a weight average molecular weight of 80000g / mol into N,N-dimethylformamide, dissolve after mechanical stirring for 90 minutes, and then add active mineral powder with a particle size of 600nm, wherein the active mineral powder It is made by mixing tourmaline, diatomite, medical stone and titanium dioxide in a mass ratio of 3:2:3:2, wherein tourmaline is a mixture of magnesium tourmaline and lithium tourmaline in a mass ratio of 6:4, and the formed mixture The mass percentage of chitosan, N,N-dimethylformamide, and active mineral powder in the solution is 0.08:0.79:0.13, and then the spinning solution is obtained after ultrasonic dispersion at a temperature of 10°C for 2 hours, and then the The spinning hole of the spinning raw material tank for centrifugal spinning is closed, wherein the diameter of the spinning hole is 1 μm, and then the spinning stock solution is slowly injected into the spinning raw material tank for centrifugal spinning, and at the s...
Embodiment 2
[0042] Add chitosan with a weight-average molecular weight of 100,000g / mol into N,N-dimethylformamide, dissolve after mechanical stirring for 90 minutes, and then add active mineral powder with a particle size of 700nm, wherein the active mineral powder It is formed by mixing tourmaline, diatomite, medical stone and titanium dioxide in a mass ratio of 3:2:3:2, wherein tourmaline is a mixture of magnesium tourmaline and lithium tourmaline in a mass ratio of 3:7, and the formed mixture Chitosan, N,N-dimethylformamide, and active mineral powder in the solution are 0.1:0.8:0.1 by mass percentage, and then the spinning solution is obtained after ultrasonic dispersion at a temperature of 20°C for 3 hours, and the centrifugal spinning solution is turned off. The spinning hole of the spinning raw material tank, wherein the diameter of the spinning hole is 10 μm, and then the spinning dope is slowly injected into the centrifugal spinning spinning raw material tank, and at the same time,...
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