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Preparing method and application of volatile limette oil

A technology of white lemon and volatile oil, which is applied in the application and preparation of tobacco, essential oils/flavors, etc., which can solve the problems of high production cost, high irritation, and low extraction rate, and achieve pure quality, clear smoke aroma, and improved extraction rate effect

Inactive Publication Date: 2018-08-28
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Natural flavorings for tobacco are popular due to their naturalness. Flavoring and adding materials as flavor compensation for low-tar cigarettes is an effective means, but the preparation methods and processes of natural flavorings still have low extraction rate, high production cost, low purity, impurities Defects such as more, more irritating, and characteristic aroma covering up cigarette aroma

Method used

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  • Preparing method and application of volatile limette oil

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Effect test

Embodiment 1

[0021] A preparation method of white lemon volatile oil, comprising the steps of:

[0022] (1) Raw material processing: After cleaning the white lemon fruit, the peel and pulp are separated, the core is removed, the peel and the pulp residue after squeezing the lemon juice are air-dried, and they are put into a low-temperature pulverizer at 2°C and pulverized into a 40-mesh coarse powder , sieve, and vacuumize the raw material powder for 15 minutes by pumping the vacuum, mix the raw material powder and water evenly according to the mass ratio of 1:50, and pour it into the extraction tank;

[0023] (2) Biotransformation: add cinnamic acid, caffeic acid (food grade, account for 0.1% of the white lemon powder mass, proportioning is 1:0.5) in the extraction tank, add compound biological agent (Lactobacillus rhamnosus (L.rhamnosus ), β-glucosidase, α-glucosidase, pectinase, limonin dehydrogenase, all of which are food grade, with enzyme activities of 2000u / g, 500u / g, 5000u / g, 20000...

Embodiment 2

[0028] A preparation method and application of white lemon volatile oil, comprising the steps of:

[0029] (1) Raw material processing: After the white lemon fruit is cleaned, the peel and pulp are separated, the core is removed, the peel and the pulp residue after squeezing the lemon juice are air-dried, and they are put into a low-temperature pulverizer at 3° C. and pulverized into 120-mesh powder. Sieve, vacuumize the raw material powder for 10 minutes by means of pumping vacuum, mix the raw material powder and water evenly according to the mass ratio of 1:35, and pour it into the extraction tank;

[0030] (2) Biotransformation: add cinnamic acid, citric acid, benzoic acid (food grade, account for 0.3% of the white lemon powder quality, proportioning is 1:2:0.5) in the extraction tank, add compound biological agent (rhamnose Lactobacillus (L.rhamnosus), β-glucosidase, α-glucosidase, pectinase, limonin dehydrogenase, all food grade, enzyme activities are 3000u / g, 1000u / g, 10...

Embodiment 3

[0035] A preparation method and application of white lemon volatile oil, comprising the steps of:

[0036] (1) Raw material processing: After the white lemon fruit is cleaned, the peel and pulp are separated, the core is removed, the peel and the pulp residue after squeezing the lemon juice are air-dried, and they are put into a low-temperature pulverizer together at 1° C. to be pulverized into 200-mesh powder. Sieve, vacuumize the raw material powder for 5 minutes by pumping it to vacuum, mix the raw material powder and water evenly according to the mass ratio of 1:10, and pour it into the extraction tank;

[0037](2) biotransformation: add cinnamic acid, caffeic acid, citrate, benzoic acid (food grade, account for 0.5% of the white lemon powder quality in the extraction tank, the proportioning between is mass ratio 1:0.6:0.4:1.2 ), adding compound biological preparations (Lactobacillus rhamnosus (L.rhamnosus), β-glucosidase, α-glucosidase, pectinase, limonin dehydrogenase, a...

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Abstract

The invention provides a preparing method and application of volatile limette oil. The preparing method includes the steps that peel and pulp of limette are separated, kernels are removed, the peel and residues obtained after a limette juice is obtained by squeezing the pulp of the limette are mixed, smashed at low temperature and subjected to vacuum pressurization for wall breaking, acid is addedfor hydrolysis, a compound biological agent is added for fermentation incubation, and after biotransformation lasts for a period of time, the volatile limette oil is extracted through steam distillation. The volatile limette oil is applied into traditional-cigarette-formula cut tobacco and novel-cigarette-tobacco atomization cut tobacco and coordinates with smoke, cigarette fragrance is clear, the fragrance is rich and natural, fruit fragrance, orange flower fragrance, round cardamom fragrance, purple perilla fragrance and grease herb cream fragrance are achieved, sweet fragrance is brought to cigarettes and tobacco, the fragrance is permeable, and the defects that when volatile limette oil extracted without biotransformation is applied into cigarettes, characteristic fragrance is remarkable, limette fragrance is prominent, and slight irritation occurs are overcome.

Description

technical field [0001] The invention relates to the technical field of cigarette additives, in particular to a preparation method and application of white lemon volatile oil. Background technique [0002] Natural flavorings for tobacco are popular due to their naturalness. Flavoring and adding materials as flavor compensation for low-tar cigarettes is an effective means, but the preparation method and process of natural flavorings still have low extraction rate, high production cost, low purity, and Defects such as more, more irritating, and the characteristic aroma covers up the aroma of cigarettes. [0003] White lemon (Citrus auran-fifolia Swingle), an angiosperm plant, the fruit contains 17 kinds of amino acids, calcium, iron, phosphorus and other minerals and multivitamins, has high beauty care and medical value, and is generally steam distilled Or cold pressed to get white lemon essential oil, with the characteristic aroma of white lemon dried fruit, fresh white lemon...

Claims

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Application Information

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IPC IPC(8): C11B9/02A24B15/30A24B3/12
CPCA24B3/12A24B15/303C11B9/02C11B9/027
Inventor 魏敏宋旭艳郭国宁李超王昊
Owner HUBEI CHINA TOBACCO IND
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