Preparation method of special slow-release fertilizer for camellia
A slow-release fertilizer and camellia technology, applied in the direction of nitrogen fertilizer, phosphate fertilizer, application, etc., can solve the problems of agricultural product quality decline, low fertilizer utilization rate, and increased production cost, and achieve the effects of improving freshness, improving soil, and saving labor costs
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Embodiment 1
[0015] The preparation method of special slow-release fertilizer for camellia comprises preparation of polyuret, preparation of polyuret slow-release fertilizer, preparation of slow-release fertilizer, and its specific steps are:
[0016] 1) Polyuret preparation: Pour dipropyl carbonate into the reaction kettle and heat up to 50°C, then add urea, potassium tert-butoxide and 2-chloroaniline, and then introduce CO 2 React at a pressure of 1.2MPa and a temperature of 130°C for 5 hours, stir and cool to room temperature, and filter to obtain polyuret. The molar ratio of the above-mentioned urea to dipropyl carbonate is 1:1. In this reaction, CO 2 And trace moisture acts as a catalyst, promotes the reaction, uses urea to indirectly chemically fix carbon dioxide, and reduces the greenhouse gas CO in the atmosphere 2 It is a kind of green synthesis process. Polyuret is a polyamide formed by linking urea molecules with carbonyl groups. It is a polyamide formed by connecting multiple a...
Embodiment 2
[0023] The preparation method of special slow-release fertilizer for camellia comprises preparation of polyuret, preparation of polyuret slow-release fertilizer, preparation of slow-release fertilizer, and its specific steps are:
[0024] 1) Polyuret preparation: Pour dipropyl carbonate into the reaction kettle and heat up to 50°C, then add urea, potassium tert-butoxide and 2-chloroaniline, and then introduce CO 2 React at a pressure of 0.8 MPa and a temperature of 140°C for 4 hours, stir and cool to room temperature, and filter to obtain polyuret. The molar ratio of the above urea to dipropyl carbonate is 2:1;
[0025] 2) Preparation of polyuret slow-release fertilizer: add dipotassium hydrogen phosphate to polyuret at a weight ratio of 1.1:1, stir and react at 80°C for 4 hours, and cool to obtain a binary intercalation of polyuret and potassium dihydrogen phosphate Segment copolymer, polyuret slow-release fertilizer;
[0026] 3) Preparation of slow-release fertilizer: Take ...
Embodiment 3
[0031] The preparation method of special slow-release fertilizer for camellia comprises preparation of polyuret, preparation of polyuret slow-release fertilizer, preparation of slow-release fertilizer, and its specific steps are:
[0032] 1) Polyuret preparation: Pour dipropyl carbonate into the reaction kettle and heat up to 50°C, then add urea, potassium tert-butoxide and 2-chloroaniline, and then introduce CO 2 React at a pressure of 1.0 MPa and a temperature of 135°C for 4.5 hours, stir and cool to room temperature, and filter to obtain polyuret. The molar ratio of the above urea to dipropyl carbonate is 1.5:1;
[0033] 2) Preparation of polyuret slow-release fertilizer: add dipotassium hydrogen phosphate to polyuret at a weight ratio of 1.15:1, stir and react at 78°C for 5 hours, and cool to obtain a binary intercalation of polyuret and potassium dihydrogen phosphate Segment copolymer, polyuret slow-release fertilizer;
[0034] 3) Preparation of slow-release fertilizer: ...
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