Preparation method and quality control method of Yulan Jiangtang capsule extract
A quality control method and Yulan hypoglycemic technology, applied in the preparation of Yulan Jiangtang capsule extract, the field of quality control of Yulan Jiangtang capsule extract, can solve the problem of insignificant effect, increased dosage, and no quality identification standard and other problems to achieve the effect of controlling product quality and improving product quality
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Embodiment 1
[0022] Embodiment 1, the preparation method of Yulan Jiangtang capsule extract
[0023] The preparation method of Yulan Jiangtang Capsule Extract comprises the following steps: get 620g of Scutellaria baicalensis, 285g of mulberry leaves, 260g of arctium burdock, 180g of blue ginseng, 170g of Scutellaria barbata, 120g of false longevity bamboo root, 93g of Qingzhizi, 30g mulberry leaves are crushed into fine powder (through 80 mesh sieve), the remaining mulberry leaves and other six flavors are decocted in boiling water twice, the first time is 2 hours, the second time is 1.5 hours, the decoctions are combined, filtered, and the filtrate is concentrated to relative The clear paste with a density of 1.17-1.20 (80°C) is ready, and the prepared clear paste is brown.
[0024] The conversion rate of baicalin can be improved by adding boiling water and decocting in the preparation process.
Embodiment 2
[0025] Embodiment 2, the quality control method of blue Jiangtang capsule extract
[0026]The quality control method of Lanjiangtang capsule extract, including baicalin identification, mulberry leaf identification, arctiin identification and baicalin content detection;
[0027] Wherein the identification of baicalin is as follows: take Yulan Jiangtang Capsule extract 1ml (respectively take 5 batch numbers for testing: T20130601-YJ, T20130602-YJ, T20130603-YJ, T20130604-YJ, T20130605-YJ), add methanol 20ml, Sonicate for 15 minutes, filter, evaporate the filtrate to dryness, add methanol 3ml to dissolve the residue, and use it as the test solution. Take another baicalin reference substance (batch number: 110715-201016, source: China Institute for the Control of Pharmaceutical and Biological Products), add methanol to make a solution containing 1mg per 1ml, and use it as the reference substance solution. According to the thin-layer chromatography (Appendix VIB of "Chinese Pharma...
Embodiment 3
[0032] (1) Selection of sample processing solvent
[0033] Accurately weigh 35.98mg of baicalin reference substance, put in a 50ml volumetric flask, add methanol to dissolve and dilute to the mark, and obtain a stock solution containing 0.6764mg per 1ml. Precisely measure 5ml of the stock solution, put it in a 50ml volumetric flask, add methanol to dissolve and dilute to the mark, and shake well to obtain a reference substance solution containing 0.06764mg per 1ml. Referring to the content determination method of the finished Yulan Jiangtang Capsules, take 10 parts of the test product (batch number: T20130607-FJ), each 1.5g, accurately weighed, put in a stoppered triangle bottle, add 25ml of methanol to No. 1 and No. 2, Add 25ml of ethanol to No. 3 and No. 4 precision, add 25ml of 75% ethanol to No. 5 and No. 6 precision, add 25ml of 70% ethanol to No. 7 and No. 8 precision, add 25ml of 65% ethanol to No. 9 and No. 10 precision, weigh the weight, and ultrasonic for 30 minutes....
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