Thermal insulation coating for buildings and preparation method of thermal insulation coating
A technology for thermal insulation coatings and construction, applied in fire-resistant coatings, epoxy resin coatings, coatings, etc., can solve the problems of poor high temperature resistance, coating peeling, restrictions, etc. The effect of good chemical temperature resistance and high temperature resistance
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Embodiment 1
[0023] The preparation method of silicon nitride / epoxy resin is:
[0024] Add epoxy resin and silicon nitride to acetone, carry out ultrasonic dispersion to obtain a dispersion liquid, raise the temperature of the dispersion liquid to 78°C, then add vinyltrioxysilane, water and polyamide in sequence, stir evenly, and dry after the reaction That's it. The mass ratio of epoxy resin to silicon nitride is 6:1, the mass ratio of vinyltrioxysilane to epoxy resin is 1:25, and the mass ratio of polyamide to silicon nitride is 1:20.
[0025] Modified rutile titanium dioxide is prepared by the following method:
[0026] Add rutile titanium dioxide to acetone, then add titanate coupling agent and stir evenly, condense and reflux for 4 hours at a temperature of 60° C. to obtain a mixture, and filter, wash and dry the mixture to obtain modified rutile titanium dioxide.
Embodiment 2
[0028] The preparation method of silicon nitride / epoxy resin is:
[0029] Add epoxy resin and silicon nitride to acetone, carry out ultrasonic dispersion to obtain a dispersion liquid, raise the temperature of the dispersion liquid to 75-82°C, then add vinyltrioxysilane, water and polyamide in sequence, stir evenly, and the reaction ends Then dry it. The mass ratio of epoxy resin to silicon nitride is 8:1, the mass ratio of vinyltrioxysilane to epoxy resin is 1:15, and the mass ratio of polyamide to silicon nitride is 1:30.
[0030] Modified rutile titanium dioxide is prepared by the following method:
[0031] Add rutile titanium dioxide to acetone, then add titanate coupling agent and stir evenly, condense and reflux for 2 hours at a temperature of 80°C to obtain a mixture, filter, wash and dry the mixture to obtain modified rutile titanium dioxide.
Embodiment 3
[0033] A heat-insulating coating for buildings, calculated in parts by weight, comprising the following components:
[0034] 45 parts of acrylic emulsion, 30 parts of silicon nitride / epoxy resin, 15 parts of potassium hexatanate whiskers, 16 parts of modified rutile titanium dioxide, 2 parts of ammonium acrylate dispersant, 0.8 parts of tetrachloroisophthalonitrile, modified 6 parts of ammonium polyacrylate, 2 parts of mineral oil, 9 parts of propylene glycol ether and 50 parts of deionized water.
[0035] Preparation:
[0036] 1) Add ammonium acrylate dispersant, tetrachloroisophthalonitrile, and 1 / 2 mineral oil into deionized water according to the formula amount, and stir and mix thoroughly at a speed of 300r / min;
[0037] 2) In the mixture of step 1), add the modified rutile type titanium dioxide of embodiment 1 and potassium hexataftate whiskers and disperse at a rotating speed of 1000r / min;
[0038] 3) Add the mixture of acrylic emulsion and silicon nitride / epoxy resin...
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