A kind of preparation method of high-frequency soft magnet silicon-aluminum magnetic powder core

Abstract

The invention discloses a method for preparing a high-frequency soft magnet silicon-aluminum magnetic powder core, belonging to the technical field of energy storage materials. In the present invention, firstly, mechanically pulverize the Fe-Si-Al alloy, then classify, and use powders of different particle sizes to gradate to obtain graded gold powder, then ultrasonically disperse the graded gold powder with absolute ethanol, polyvinylpyrrolidone and dopamine, React under protected state to prepare graded gold powder slurry, then add tetraethyl orthosilicate diluent dropwise to graded gold powder slurry, after the dropwise addition is complete, add catalyst, stir and mix before adding ethanol solution, continue to stir and react, and then filter, wash and dry to obtain modified alloy powder; then mix and dry the modified alloy powder and insulating binder, add a release agent, injection molding, and demoulding. Afterwards, it undergoes stabilization treatment, heat treatment, and cooling to obtain a high-frequency soft magnet silicon-aluminum magnetic powder core.

Description

technical field

[0001] The invention discloses a preparation method of a silicon-aluminum magnetic powder core of a high-frequency soft magnet, belonging to the technical field of energy storage materials. Background technique

[0002] As a soft magnetic alloy material with excellent magnetic properties, sendust not only has high hardness, high resistivity, low magnetic anisotropy constant, low coercive force, low hysteresis loss and low eddy current loss, but also has extremely strong Corrosion resistance is also widely used as a structural material. It is a new type of electronic energy-saving material. The sendust magnetic powder core is based on the powder metallurgy process. It is coated with sendust powder through surface insulation and bonded It is a soft magnetic material made by mixing and pressing agents. In recent years, the application of soft magnetic silicon aluminum powder and its magnetic powder core products in the electronics industry has received great at...

Examples

example 1

[0022]Put the sendust in the pulverizer, after mechanical crushing, use a 500-mesh round hole screen to classify, and carry out grading according to the following weight parts, 200 mesh accounts for 15 parts, 325 mesh accounts for 35 parts, and 500 mesh accounts for 75 parts. to obtain graded gold powder; mix graded gold powder and absolute ethanol at a mass ratio of 1:10 and pour it into a three-necked flask. Under the condition of an ultrasonic frequency of 50 kHz, ultrasonically disperse it for 60 minutes, and then add graded gold powder into the three-necked flask. Polyvinylpyrrolidone with 0.8 times the mass of gold powder and dopamine with 0.03 times the mass of graded gold powder were continued to be ultrasonically dispersed at a frequency of 50 kHz for 60 minutes, and then the ultrasonic wave was stopped. Feed nitrogen into the three-necked flask at a high rate, under nitrogen protection, at a temperature of 70°C and a rotation speed of 500r / min, heat and stir at a cons...

example 2

[0024] Put the sendust in the pulverizer, after mechanical crushing, use a 500-mesh round hole screen to classify, and carry out grading according to the following weight parts, 200 mesh accounts for 15 parts, 325 mesh accounts for 35 parts, and 500 mesh accounts for 75 parts. to obtain graded gold powder; mix graded gold powder and absolute ethanol at a mass ratio of 1:10 and pour it into a three-necked flask. Under the condition of an ultrasonic frequency of 50 kHz, ultrasonically disperse it for 60 minutes, and then add graded gold powder into the three-necked flask. Polyvinylpyrrolidone with 0.8 times the mass of gold powder and dopamine with 0.03 times the mass of graded gold powder were continued to be ultrasonically dispersed at a frequency of 50 kHz for 60 minutes, and then the ultrasonic wave was stopped. Nitrogen gas was passed into the three-necked flask at a high rate, under the condition of nitrogen protection, at a temperature of 70°C and a rotation speed of 500r / ...

example 3

[0026] Put the sendust in the pulverizer, after mechanical crushing, use a 500-mesh round hole screen to classify, and carry out grading according to the following weight parts, 200 mesh accounts for 15 parts, 325 mesh accounts for 35 parts, and 500 mesh accounts for 75 parts. to obtain graded gold powder; mix graded gold powder and absolute ethanol at a mass ratio of 1:10 and pour it into a three-necked flask. Under the condition of an ultrasonic frequency of 50 kHz, ultrasonically disperse it for 60 minutes, and then add graded gold powder into the three-necked flask. Polyvinylpyrrolidone with a mass of 0.8 times the gold powder was dispersed ultrasonically for 60 minutes at a frequency of 50 kHz, then the ultrasonic was stopped, and the three-necked flask was moved into a digital display speed measuring constant temperature magnetic stirrer, and nitrogen gas was introduced into the three-necked flask at a rate of 8 mL / min. Under nitrogen protection, at a temperature of 70°C ...

technical field

[0001] The invention discloses a preparation method of a silicon-aluminum magnetic powder core of a high-frequency soft magnet, belonging to the technical field of energy storage materials. Background technique

[0002] As a soft magnetic alloy material with excellent magnetic properties, sendust not only has high hardness, high resistivity, low magnetic anisotropy constant, low coercive force, low hysteresis loss and low eddy current loss, but also has extremely strong Corrosion resistance is also widely used as a structural material. It is a new type of electronic energy-saving material. The sendust magnetic powder core is based on the powder metallurgy process. It is coated with sendust powder through surface insulation and bonded It is a soft magnetic material made by mixing and pressing agents. In recent years, the application of soft magnetic silicon aluminum powder and its magnetic powder core products in the electronics industry has received great at...

Examples

example 1

[0022]Put the sendust in the pulverizer, after mechanical crushing, use a 500-mesh round hole screen to classify, and carry out grading according to the following weight parts, 200 mesh accounts for 15 parts, 325 mesh accounts for 35 parts, and 500 mesh accounts for 75 parts. to obtain graded gold powder; mix graded gold powder and absolute ethanol at a mass ratio of 1:10 and pour it into a three-necked flask. Under the condition of an ultrasonic frequency of 50 kHz, ultrasonically disperse it for 60 minutes, and then add graded gold powder into the three-necked flask. Polyvinylpyrrolidone with 0.8 times the mass of gold powder and dopamine with 0.03 times the mass of graded gold powder were continued to be ultrasonically dispersed at a frequency of 50 kHz for 60 minutes, and then the ultrasonic wave was stopped. Feed nitrogen into the three-necked flask at a high rate, under nitrogen protection, at a temperature of 70°C and a rotation speed of 500r / min, heat and stir at a cons...

example 2

[0024] Put the sendust in the pulverizer, after mechanical crushing, use a 500-mesh round hole screen to classify, and carry out grading according to the following weight parts, 200 mesh accounts for 15 parts, 325 mesh accounts for 35 parts, and 500 mesh accounts for 75 parts. to obtain graded gold powder; mix graded gold powder and absolute ethanol at a mass ratio of 1:10 and pour it into a three-necked flask. Under the condition of an ultrasonic frequency of 50 kHz, ultrasonically disperse it for 60 minutes, and then add graded gold powder into the three-necked flask. Polyvinylpyrrolidone with 0.8 times the mass of gold powder and dopamine with 0.03 times the mass of graded gold powder were continued to be ultrasonically dispersed at a frequency of 50 kHz for 60 minutes, and then the ultrasonic wave was stopped. Nitrogen gas was passed into the three-necked flask at a high rate, under the condition of nitrogen protection, at a temperature of 70°C and a rotation speed of 500r / ...

example 3

[0026] Put the sendust in the pulverizer, after mechanical crushing, use a 500-mesh round hole screen to classify, and carry out grading according to the following weight parts, 200 mesh accounts for 15 parts, 325 mesh accounts for 35 parts, and 500 mesh accounts for 75 parts. to obtain graded gold powder; mix graded gold powder and absolute ethanol at a mass ratio of 1:10 and pour it into a three-necked flask. Under the condition of an ultrasonic frequency of 50 kHz, ultrasonically disperse it for 60 minutes, and then add graded gold powder into the three-necked flask. Polyvinylpyrrolidone with a mass of 0.8 times the gold powder was dispersed ultrasonically for 60 minutes at a frequency of 50 kHz, then the ultrasonic was stopped, and the three-necked flask was moved into a digital display speed measuring constant temperature magnetic stirrer, and nitrogen gas was introduced into the three-necked flask at a rate of 8 mL / min. Under nitrogen protection, at a temperature of 70°C ...

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