A kind of antibacterial far-infrared health-care quick-drying nylon fiber and its preparation method and application
A far-infrared health care and nylon fiber technology, which is applied in the field of fiber processing, can solve the problems of limited volume of Taichi stone nano-powder, Taichi stone fiber/silk thread can not play well the far-infrared and antibacterial effects of Taichi stone, and achieve far-infrared Effective, cost-effective, simple treatment
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Embodiment 1
[0033] A preparation method for antibacterial far-infrared health-care quick-drying nylon fiber, which comprises the following steps:
[0034] (1) Preparation of fluorine-containing silicone treatment solution for Taiji stone. Take a certain amount of heptadecafluorodecyltriethoxysilane and put it into a clean container, add an appropriate amount of isopropanol solvent to dilute it for use, so that the volume of the heptadecafluorodecyltriethoxysilane dilution is 100mL , the mass fraction is 5%.
[0035](2) Surface modification of Taichi stone nanopowder. Disperse 10g of commercially available Taichi stone nanopowder in the heptadecafluorodecyltriethoxysilane diluent prepared in the above step (1), fully stir and disperse, add formic acid dropwise to adjust the pH to 3, and then disperse by ultrasonic wave for 120min After dispersing and mixing evenly, stir and react at 40°C for 6 hours. Heptadecafluorodecyltriethoxysilane will undergo hydrolysis reaction in the solution, in...
Embodiment 2
[0038] A preparation method for antibacterial far-infrared health-care quick-drying nylon fiber, which comprises the following steps:
[0039] (1) Preparation of fluorine-containing silicone treatment solution for Taiji stone. Take a certain amount of heptadecafluorodecyltriisopropoxysilane and put it into a clean container, add an appropriate amount of isopropanol solvent to dilute it for use, so that the volume of the heptadecafluorodecyltriisopropoxysilane dilution It is 120mL, and the mass fraction is 3%.
[0040] (2) Surface modification of Taichi stone nanopowder. Disperse 10 g of commercially available Taichi stone nanopowder after the surface is fully dried in the heptadecafluorodecyltriisopropoxysilane diluent prepared in the above step (1), fully stir and disperse, add acetic acid dropwise to adjust the pH to 4, Then ultrasonically disperse for 60 minutes, disperse and mix evenly, and then stir and react at 30°C for 4 hours. Heptadecafluorodecyltriisopropoxysilane ...
Embodiment 3
[0043] A preparation method for antibacterial far-infrared health-care quick-drying nylon fiber, which comprises the following steps:
[0044] (1) Preparation of fluorine-containing silicone treatment solution for Taiji stone. Take a certain amount of tridecafluorooctyltriethoxysilane and put it into a clean container, add an appropriate amount of absolute ethanol solvent to dilute it for use, so that the volume of tridecafluorooctyltriethoxysilane dilution is 100mL , the mass fraction is 3%.
[0045] (2) Surface modification of Taichi stone nanopowder. Disperse 10 g of commercially available Taichi stone nanopowder in the diluted solution of tridecafluorooctyltriethoxysilane prepared in the above step (1) after the surface is fully dried, fully stir and disperse, add acetic acid dropwise to adjust the pH to 4, and then Then ultrasonically disperse for 70 minutes, disperse and mix evenly, and then stir and react at 50°C for 4 hours. Between oxane molecules and between silox...
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