Preparation method of seawater corrosion resistant wear-resistant composite coating
A composite coating, corrosion and wear technology, applied in the direction of coating, metal material coating process, fusion spray plating, etc., can solve the problems of reliability, safety and service life of mechanical parts, and achieve improved bonding strength, excellent The effect of corrosion and wear resistance
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[0032] A seawater corrosion and wear resistant NiAl-Cr of the present invention 2 o 3 -The preparation method of Mo composite coating, by adding Cr 2 o 3 and Mo, the microhardness of the composite coating increased from 195.1HV to 362.3HV, the friction coefficient in seawater environment decreased from 0.29 to 0.26, and the wear rate decreased from 3.2×10 -5 mm 3 / N.m reduced to 2.7×10 -5 mm 3 / N.m, the corrosion and wear performance of the coating in the seawater environment is significantly improved, and the composite coating shows excellent comprehensive performance; the specific steps are as follows:
[0033] S1, mixed powder
[0034] In terms of mass fraction, NiAl is 60-75%, Cr 2 o 3 Mo is 15-25%, Mo is 10-15%, and the powder is mixed evenly on a three-dimensional powder mixer;
[0035] S2, grinding the surface of the base sample;
[0036]Grind the cut base sample on coarse sandpaper to remove the remaining oil stains on the surface of the base sample; select I...
Embodiment 1
[0048] The spraying tests were carried out using the laboratory's SulZer Metco 9M plasma spraying apparatus. Firstly, in terms of mass fraction, NiAl is 60-75%, Cr 2 o 3 15% to 25% Mo, 10% to 15% Mo, mix the weighed powder evenly on a three-dimensional powder mixer, and dry the evenly mixed spray powder in a vacuum drying oven to ensure smooth powder delivery during the spraying process , and then sandblasting and cleaning the base material to remove oil stains and sand remaining on the base surface. Before spraying, the substrate material should be preheated to reduce the temperature difference between the molten particles and the substrate surface, so that it can better adhere to the substrate surface, thereby improving the bonding strength of the coating. After the substrate sample is preheated to 300 At ~500°C, carry out the spraying test. The spraying parameters during the test are Ar flow rate 38-45L / min, H 2 The flow rate is 4.5-6L / min, the spraying angle is 80-100°...
Embodiment 2
[0050] The coating prepared in Example 1 was cut into a corrosion wear test sample, the sample size was 20mm × 20mm × 1.5mm, the corrosion solution was artificial seawater, and the artificial seawater was proportioned according to the ASTMD114-98 standard, with 0.1M NaOH solution Adjust the pH value of the artificial seawater to 8.2. Before the test, the sample was soaked in the solution tank for 0.5 hours, and then the corrosion and wear test was carried out on the corrosion and wear testing machine. The friction speed is 0.8mm / s, the force is 5N, the reciprocating friction test range is 3.5mm, and the friction test is 1 hour. Measured by adding Cr 2 o 3 and Mo, the friction coefficient of the coating decreased from 0.29 to 0.26, and the wear rate decreased from 3.2×10 -5 mm 3 / N.m reduced to 2.7×10 -5 mm 3 / N.m, the corrosion resistance and wear resistance are significantly enhanced, such as Figure 4 , 5 shown.
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