Anti-blue ray/color-changing bifunctional optical resin material and preparation method thereof

An optical resin, anti-blue light technology, applied in the field of light absorbing materials, can solve problems such as damage, and achieve the effect of good effect, good anti-blue light, and enhanced mutual synergy

Inactive Publication Date: 2019-02-22
南京米兰达视光科学研究院有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be widely used in automobile windows, optical protective glass, LED light protective film, mobile phone protective screen, eye protection equipment and other fields to solve the damage caused by harmful light to human eyes

Method used

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  • Anti-blue ray/color-changing bifunctional optical resin material and preparation method thereof
  • Anti-blue ray/color-changing bifunctional optical resin material and preparation method thereof
  • Anti-blue ray/color-changing bifunctional optical resin material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] Example 1: Preparation of anti-blue light nanocomposite microspheres, anti-blue light coating solution, anti-blue light optical glass, anti-blue light / color-changing dual-function optical glass and anti-blue light / color-changing dual-function optical resin material

[0053] (1) Preparation of anti-blue light nanocomposite microspheres:

[0054] 1. Add 80g of sodium acetate to 1000g of pure water, gradually raise the temperature to 100°C, after turning into a transparent sodium acetate aqueous solution, add 130g of nano-titanium oxide, stir for 20 minutes, cool to room temperature, the reaction solution gradually precipitates in layers, and solid-liquid filtration After separation and washing, add 1500g of ethanol, then stir and add 50g of ultraviolet absorber UV-P, stir for 20 minutes, let stand for 50 minutes, filter and collect the precipitate, and dry to obtain titanium oxide modified nanomaterials;

[0055] Figure 5 It is the transmission electron microscope TEM i...

Embodiment 2

[0074] Example 2: Preparation of anti-blue light nanocomposite microspheres, anti-blue light coating solution, anti-blue light optical glass, anti-blue light / color-changing dual-function optical glass and anti-blue light / color-changing dual-function optical resin material

[0075] (1) Preparation of anti-blue light nanocomposite microspheres:

[0076] Add 95g of sodium acetate to 1000g of pure water, gradually raise the temperature to 100°C, after turning into a transparent sodium acetate aqueous solution, add 180g of nano-titanium oxide, stir for 20 minutes, cool to room temperature, the reaction solution is gradually layered and precipitated, separated by solid-liquid filtration, After washing, add 1700g of ethanol, then stir and add 36g of ultraviolet absorber UV-P, stir for 25 minutes, let stand for 50 minutes, filter and collect the precipitate, dry to obtain titanium oxide modified nanomaterials;

[0077] Take 7g titanium oxide modified nanomaterials, 4.2g isophorone dii...

Embodiment 3

[0087] Example 3: Preparation of anti-blue light nanocomposite microspheres, anti-blue light coating solution, anti-blue light optical glass, anti-blue light / color-changing dual-function optical glass and anti-blue light / color-changing dual-function optical resin material

[0088] (1) Preparation of anti-blue light nanocomposite microspheres:

[0089] Add 75g of sodium acetate to 1000g of pure water, gradually raise the temperature to 100°C, after turning into a transparent sodium acetate aqueous solution, add 100g of nano-titanium oxide, stir for 20 minutes, cool to room temperature, the reaction solution is gradually layered and precipitated, separated by solid-liquid filtration, After washing, add 1300g of ethanol, then stir and add 28g of ultraviolet absorber UV-P, stir for 20 minutes, let stand for 50 minutes, filter and collect the precipitate, and dry to obtain titanium oxide modified nanomaterials;

[0090] Take 7g of titanium oxide modified nanomaterials, 7g of m-xyly...

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Abstract

The invention discloses an anti-blue ray/color-changing bifunctional optical resin material and a preparation method thereof. The bifunctional optical resin material is composed of an anti-blue ray optical resin material and a photochromic coating coated on the material surface. The anti-blue ray optical resin material is prepared by dispersing polyurethane/light absorber/titanium oxide nanocomposite microspheres in a polyurethane optical resin. The nanocomposite microspheres are of a three-layer composite core-shell structure, the core refers to titanium oxide nano microspheres, the middle layer refers to a light absorber, and the shell is polyurethane. The spectrum blocking range of the anti-blue ray optical resin material is expanded from an ultraviolet spectrum region to a blue-ray spectrum region, and the anti-blue ray optical resin material has distinguished absorption performance on blue rays of different bands on the premise of ensuring high transmittance. The anti-blue ray optical resin material and the photochromic coating are subjected to matching and function integration, the transmittance can be automatically regulated according to light intensity, darkness control isrealized by selectively transmitting beneficial light and cutting off harmful light, and light transmission is performed according to needs.

Description

technical field [0001] The invention belongs to the technical field of light-absorbing materials, and in particular relates to an optical material with specific absorption for different wavelengths in the 280-450nm spectral region and a preparation method thereof. Background technique [0002] As we all know, ultraviolet rays can damage human eyes. In addition, blue light in visible light can also cause damage to eyes. As part of visible light, blue light has extremely high energy, and its wavelength range is between 400 and 500nm. With the widespread popularization of electronic products such as computers, mobile phones, and ipads, unnatural light with blue light as the main body will cause irreversible damage to human eyes. Damage, causing dry eyes, fatigue, tearing, accelerated myopia, macular area disease and other problems. According to the orange warning issued by the World Health Organization (WHO) at the end of 2009: the potential invisible threat of blue light to h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J7/04B01J13/14C08G18/66C08G18/48C08G18/32C08K9/10C08K3/22C03C17/32C08L75/04
CPCB01J13/14C03C17/322C08G18/3206C08G18/4854C08G18/6674C08J2375/04C08J2475/08C08K3/22C08K9/10C08K2003/2241C08K2201/011C08J7/0427
Inventor 张鹤军邹永存张凌乔振安王明华沈秋雨纪立军范为正司云凤刘洋郑永华
Owner 南京米兰达视光科学研究院有限公司
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